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A series of N-protected 1-aminoalkylphosphonate mixed monothioesters and dithioesters were synthesized using onepot reactions of benzyl carbamate, aldehydes and alkoxyphosphine dichlorides or alkylthiophosphine dichloride, followed by alcoholysis with thiol or alcohols in the presence of triethylamine.
This project was supported by NSFC.
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