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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 15
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Original Articles

A CONVENIENT AND MILD PROCEDURE FOR THE PREPARATION OF α-KETO PHOSPHONATES OF 1-HYDROXYPHOSPHONATES UNDER SOLVENT-FREE CONDITIONS USING MICROWAVE

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Pages 2245-2250 | Received 06 Jul 2000, Published online: 09 Nov 2006
 

Abstract

The Reactions of 1-hydroxyphosphonates on the alumina-supported CrO3 are accelerated by microwave irradiation under solvent-free conditions to afford a high yielding synthesis of α-keto phosphonates.

ACKNOWLEDGMENT

The Institute for Advanced Studies in Basic Sciences (IASBS) is thanked for supporting the work.

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