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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 15
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Original Articles

FACILE SYNTHESIS OF 1,3-DICHLOROTETRAORGANODISILAZANES

Cai-Hong Xu Center for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100080, China
,
Zhi-Min Zheng Center for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100080, China
,
Yong-Ming Li Center for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100080, China
,
Zhi-Jie Zhang Center for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100080, China
&
Ze-Min Xie Center for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100080, China
Pages 2271-2275 | Received 25 Jul 2000, Published online: 09 Nov 2006
 
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Abstract

A new 1,3-dichlorodisilazane, 1,3-dichloro-1,3-dimethyl-1,3-divinyldisilazane (DMDV), was prepared from the trans-silylation reaction of hexamethyldisilazane (MMN) and methylvinyldichlorosilane. The reactions between MMN and other dichlorosilanes, R2SiCl2 (R = Me, Ph) in the absence of catalyst were also investigated, and the expected, 1,3-dichlorosilazanes, (ClSiMe2)2NH and (ClSiPh2)2NH were obtained, respectively.

Acknowledgments

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