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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 16
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Original Articles

SYNTHESIS AND REACTIONS OF SOME 1,2,4-TRIAZOLO-[4,3-b]-1,2,4-TRIAZOLES

, , &
Pages 2447-2456 | Received 10 Nov 2000, Published online: 09 Nov 2006
 

Abstract

Reaction of 5-aryl-3-chloro-4-phenyl-1,2,4-triazoles (1 & 2) with hydrazine hydrate afforded the hydrazino derivatives 3 and 4. Reaction of 3 and 4 with carboxylic acids, CS2 and phenylisothiocyanate gave the s-triazole-fused ring systems 512. On the other hand, reaction of 3 and 4 with nitrous acid gave tetrazole-fused ring systems 13 and 14, respectively. Mannich reaction on compounds 9 and 10 afforded Mannich bases 15 and 16.

Acknowledgments

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