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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 19
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Original Articles

ASYMMETRIC TRIMETHYLSILYL-CYANATION OF ALDEHYDES CATALYZED BY CHIRAL SCHIFF BASE-Ti(OiPr)4 COMPLEX

Zhuohong Yang State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300 071, P. R. China
,
Zhenghong Zhou State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300 071, P. R. China
&
Chuchi Tang State Key Laboratory of Elemento-Organic Chemistry, Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300 071, P. R. China
Pages 3031-3036 | Received 12 Oct 2000, Published online: 16 Aug 2006
 
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Abstract

A new chiral Schiff base 4 was synthesized, which was found to be efficient catalyst for the enantioselective silylcyanation of aldehydes. The enantioselectivities of 25.1–72.7% were obtained by using the chiral Schiff base-Ti(OiPr)4 complex.

ACKNOWLEDGMENT

We are grateful to the National Science Foundation (No. 29872016) for generous financial support.

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