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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 20
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Original Articles

A ONE-STEP PROTOCOL FOR THE N-CHLOROMETHYLATION OF HETEROCYCLIC IMIDES

Shu He Department of Chemistry, Wichita State University, Wichita, Kansas, 67260, U.S.A.
,
Hongyi Yu Department of Chemistry, Wichita State University, Wichita, Kansas, 67260, U.S.A.
,
Qinghong Fu Department of Chemistry, Wichita State University, Wichita, Kansas, 67260, U.S.A.
,
Rongze Kuang Department of Chemistry, Wichita State University, Wichita, Kansas, 67260, U.S.A.
,
Jeff B. Epp Department of Chemistry, Wichita State University, Wichita, Kansas, 67260, U.S.A.
&
William C. Groutas Department of Chemistry, Wichita State University, Wichita, Kansas, 67260, U.S.A.
Pages 3055-3058 | Received 04 Dec 2000, Published online: 16 Aug 2006
 
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Abstract

A convenient single step methodology for the N-chloromethylation of heterocyclic imides using a mixture of formaldehyde sodium bisulfite adduct and thionyl chloride is described.

ACKNOWLEDGMENT

Financial support of this work by the National Institutes of Health (HL 57788) is gratefully acknowledged.

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