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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 20
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Original Articles

A CONVENIENT SYNTHESIS OF 1,3-DISUBSTITUTED-4-(1′,3′-DITHIOLANE/DITHIANE-2′-YLIDENE)-2-PYRAZOLIN-5-ONES

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Pages 3175-3181 | Received 12 Jun 2000, Published online: 16 Aug 2006
 

Abstract

1, 3 - Disubstituted- 4 - (1′, 3′- dithiolane /dithiane - 2′- ylidene) - 2 -pyrazolin-5-one derivatives like (1ac), (2ac), (3ac) have been obtained by condensation of 2-pyrazolin-5-ones (1), (2) and (3) with carbon disulfide in presence of triethylamine followed by the reaction with 1,2-dibromoethane (4a), 1,3-dibromopropane (4b) and 1,3-dibromobutane (4c) respectively.

ACKNOWLEDGMENT

The authors are thankful to Council of Scientific and Industrial Research (CSIR), New Delhi, India for the financial help.

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