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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 3
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Original Articles

A SIMPLE LARGE SCALE SYNTHESIS OF 1,3-BIS-(4,4-DIMETHYL-2-OXAZOLINYL)BENZENEFootnote1*

Karen M. Button The David Upton Hill Laboratories of Inorganic Chemistry, Department of Chemistry, Acadia University, Elliott Hall, Wolfville, Nova Scotia, B0P 1X0, Canada
,
Robert A. Gossage The David Upton Hill Laboratories of Inorganic Chemistry, Department of Chemistry, Acadia University, Elliott Hall, Wolfville, Nova Scotia, B0P 1X0, CanadaCorrespondence[email protected]
&
Ralph K. R. Phillips The David Upton Hill Laboratories of Inorganic Chemistry, Department of Chemistry, Acadia University, Elliott Hall, Wolfville, Nova Scotia, B0P 1X0, Canada
Pages 363-368 | Received 19 Mar 2001, Published online: 16 Aug 2006
 
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ABSTRACT

A simple “one-pot” procedure for the large scale and high yield synthesis of the title ligand (1) is presented which involves Lewis acid catalysed formation of 1 from 1,3-dicyanobenzene followed by a simple recrystallisation step.

*Oxazoline Chemistry: Part I.

ACKNOWLEDGMENTS

This work was made possible by the support of Acadia University and the Nova Scotia Human Resources Student Summer Placement Program. The authors are indebted to the Atlantic Regional Nuclear Magnetic Resonance Centre for NMR spectra.

Notes

*Oxazoline Chemistry: Part I.

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