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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 3
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Original Articles

A NEW AND RAPID N-ALKYLATION OF 3,6-EPOXY-HEXAHYDROPHTHALIMIDES

Guifa Su Department of Chemistry & Chemical Engineering, Guangxi Normal University, Guilin, 541004, P. R. China
,
Xinsheng Li Department of Chemistry & Chemical Engineering, Guangxi Normal University, Guilin, 541004, P. R. China
&
Hongjing Wan Department of Chemistry & Chemical Engineering, Guangxi Normal University, Guilin, 541004, P. R. China
Pages 381-385 | Received 19 Mar 2001, Published online: 16 Aug 2006
 
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ABSTRACT

Rapid N-alkylation of 3,6-epoxyhexahydrophthalimides with a series of halides were performed under solvent-free conditions coupled with microwave irradiation. The isolated yield of N-substituted 3,6-epoxyhexahydrophthalimides varied from 82 to 98%.

ACKNOWLEDGMENT

The authors are grateful to Guangxi Government for financial grants.

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