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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 6
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Original Articles

PALLADIUM-CATALYZED ELECTROCHEMICAL CARBONYLATION OF ALKYNES UNDER VERY MILD CONDITIONS

I. Chiarotto Dipartimento di Ingegneria Chimica dei Materiali delle Materie Prime e Metallurgia, Università degli Studi “La Sapienza,”, via Castro Laurenziano 7, Rome, I 00185, Italy
&
I. Carelli Dipartimento di Ingegneria Chimica dei Materiali delle Materie Prime e Metallurgia, Università degli Studi “La Sapienza,”, via Castro Laurenziano 7, Rome, I 00185, Italy
Pages 881-886 | Received 23 Mar 2001, Published online: 16 Aug 2006
 
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ABSTRACT

Terminal alkynes were carbonylated under very mild conditions to yield acetylenecarboxylates under atmospheric pressure of carbon monoxide at room temperature using palladium(II) catalyst in combination with its anodic recycling at a graphite electrodes.

ACKNOWLEDGMENTS

This work has been supported by the Consiglio Nazionale Delle Ricerche (CNR, Italy), the Ministero dell’Università e della Ricerca Scientifica e Technologica (MURST, Italy). We want to thank Dr. Anny Jutand for helpful discussions and Mr. Marco Di Pilato for his technical contribution.

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