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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 6
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Original Articles

A RAPID SYNTHESIS OF N-ARYL PHTHALIMIDES UNDER MICROWAVE IRRADIATION IN THE ABSENCE OF SOLVENT

Hui-Zhang Li College of Chemistry and Environmental Science, Hebei University, Baoding, 071002, P.R. ChinaCorrespondence[email protected]
,
Jin-Song Zhang College of Chemistry and Environmental Science, Hebei University, Baoding, 071002, P.R. China
,
Ya-Ming Zhou College of Chemistry and Environmental Science, Hebei University, Baoding, 071002, P.R. China
&
Tong-Shuang Li College of Chemistry and Environmental Science, Hebei University, Baoding, 071002, P.R. China
Pages 927-930 | Received 23 Mar 2001, Published online: 16 Aug 2006
 
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ABSTRACT

A mixture of phthalic anhydride (1) and aromatic amines (2a–h) were irradiated in a microwave oven for 2–10 min to provide N-aryl phthalimides (3a–h) in 91–95% yields.

ACKNOWLEDGMENT

The project was supported by Natural Science Foundation of Hebei Province.

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