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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 13
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Original Articles

A HIGH YIELDING, REPRODUCIBLE SYNTHESIS OF TRIMETHYLSILYLKETENE

T. Howard Black Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920, U.S.A.Correspondence[email protected]
,
John R. Farrell Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920, U.S.A.
,
Donald A. Probst Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920, U.S.A.
&
Michael C. Zotz Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920, U.S.A.
Pages 2083-2088 | Received 24 Jul 2001, Published online: 16 Aug 2006
 
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ABSTRACT

A two-step sequence for the preparation of trimethylsilylketene, from chloroacetaldehyde diethyl acetal via ethoxyacetylene, has been modified and optimized.

ACKNOWLEDGMENTS

We gratefully thank the National Institutes of Health (R15-GM52677-01), the Research Corporation, and the Council for Faculty Research of Eastern Illinois University, for their generous support of this work.

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