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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 15
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Original Articles

SOLVENT-FREE SYNTHESES OF SALICYLALDIMINES ASSISTED BY MICROWAVE IRRADIATION

Haijian Yang State Key Laboratory of Engineering Plastics and The Center for Molecular Science, Institute of Chemistry, The Chinese Academy of Sciences, Beijing, 100080, China
,
Wen-Hua Sun State Key Laboratory of Engineering Plastics and The Center for Molecular Science, Institute of Chemistry, The Chinese Academy of Sciences, Beijing, 100080, ChinaCorrespondence[email protected]
,
Zilong Li State Key Laboratory of Engineering Plastics and The Center for Molecular Science, Institute of Chemistry, The Chinese Academy of Sciences, Beijing, 100080, China
&
Leyong Wang State Key Laboratory of Engineering Plastics and The Center for Molecular Science, Institute of Chemistry, The Chinese Academy of Sciences, Beijing, 100080, China
Pages 2395-2402 | Received 04 Jun 2001, Published online: 16 Aug 2006
 
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ABSTRACT

A microwave-assisted condensation of salicylaldehyde and aryl amines without solvent were efficiently performed to form a series of salicylaldimines in high yields, which were confirmed by IR, 1H NMR, 13C NMR and elemental analyses. The microwave-assisted condensation provided a convenient environmental-friendship methodology for syntheses of Schiff-base in organic syntheses.

ACKNOWLEDGMENTS

We are grateful for the financial supports from the Chinese Academy of Sciences under Core Research for Engineering innovation KGCX203-2 and Fund of “One Hundred Talent” for WHSun.

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