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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 19
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Original Articles

A SIMPLE AND EFFICIENT PREPARATION OF (ARYLPHOSPHINYL)-METHYLPHOSPHONATES

George P. Luke Neurogen Corporation, 35 Northeast Industrial Road, Branford, CT, 06405, U.S.A.Correspondence[email protected]
&
William C. Shakespeare ARIAD Pharmaceuticals, Inc., 26 Landsdowne Street, Cambridge, MA, 02139-4234, U.S.A.
Pages 2951-2957 | Received 04 Oct 2001, Published online: 16 Aug 2006
 
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ABSTRACT

A simple and efficient preparation of (arylphosphinyl)methylphosphonates is described whereby the phosphinylmethylphosphonate group is introduced via the Pd(0) mediated phosphinylation of an aryl halide or triflate with diethyl (ethoxyphosphinyl)methylphosphonate.

Acknowledgments

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