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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 1
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Original Articles

A Convenient Synthesis of 1-Alkyl-1-phenylhydrazines from N-Aminophthalimide

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Pages 87-98 | Received 07 Aug 2001, Published online: 20 Aug 2006
 

Abstract

N-Alkylaminophthalimides were synthesized by condensation of N-aminophthalimide with aldehydes, and subsequent reduction of the intermediate with pyridine-borane in acetic acid. N-Phenylation and removal of the phthalimide group gave 1-alkyl-1-phenylhydrazines in high yield.

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