Studies on Bromination of Active Methylene by a Mixture of Hydrobromic Acid and Hydrogen Peroxide (or TBHP)

Vasudha H. Tillu Division of Organic Chemistry: Technology, National Chemical Laboratory, Pune, India

Popat D. Shinde Division of Organic Chemistry: Technology, National Chemical Laboratory, Pune, India

Ashutosh V. Bedekar Division of Organic Chemistry: Technology, National Chemical Laboratory, Pune, India

Radhika D. Wakharkar Division of Organic Chemistry: Technology, National Chemical Laboratory, Pune, IndiaCorrespondence[email protected]

Abstract

Studies on bromination of active methylene with a mixture of hydrogen peroxide or tert-butylhydroperoxide (TBHP) and hydrobromic acid are discussed. Substituted acetophenones, benzocyclic ketones provide α-bromo-keto compounds in high yields under this reaction condition.

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Acknowledgment

A. V. B. and P. D. S. wish to thank CSIR New Delhi for the award of Pool Officership and Senior Research Fellowship, respectively.

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Studies on Bromination of Active Methylene by a Mixture of Hydrobromic Acid and Hydrogen Peroxide (or TBHP)

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Studies on Bromination of Active Methylene by a Mixture of Hydrobromic Acid and Hydrogen Peroxide (or TBHP)

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