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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 12
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Original Articles

Conversion of Alkynes into α,α-Dichloro Ketones and α,α-Dichlorodimethyl Ketals Using Trichloroisocyanuric Acid

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Pages 1997-2002 | Received 17 Oct 2002, Published online: 17 Aug 2006
 

Abstract

Trichloroisocyanuric acid reacts with alkynes in the presence of water in acetone or acetonitrile to form α,α-dichloro ketones and in methanol to form α,α-dichlorodimethyl ketals.

Acknowledgment

HRMS data was provided courtesy of John R. Carney. This research was supported in part by NSF-REU program grants.

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