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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 20
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Original Articles

Robinson's Annelation: Synthesis of Sydnone-Containing 3′-Arylcyclohexenone Derivatives Under Solvent Free Conditions

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Pages 3589-3595 | Published online: 15 Aug 2006
 

Abstract

3-Aryl-4-(6′-carbethoxy-5′-arylcyclohex-2′-enone-3′-yl)sydnones 2a–i were prepared following Robinson's annelation by grinding chalcones 1a–i and ethylacetoacetate in the presence of potassium carbonate under solvent-free conditions.

Acknowledgments

The authors thank Head, RSIC, Chandigarh, and CDRI, Lucknow, for spectral and analytical data.

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