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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 1
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Original Articles

One Pot Synthesis of Monoalkylated and Mixed, Dialkylated Meldrum's Acid Derivatives

Uday V. Desai Department of Chemistry, Shivaji University, Kolhapur, 416 004, IndiaCorrespondence[email protected]
,
D. M. Pore Department of Chemistry, Shivaji University, Kolhapur, 416 004, India
,
R. B. Mane Department of Chemistry, Shivaji University, Kolhapur, 416 004, India
,
S. B. Solabannavar Department of Chemistry, Shivaji University, Kolhapur, 416 004, India
&
P. P. Wadgaonkar Polymer Division, National Chemical Laboratory, Pune, India
Pages 25-32 | Received 15 Jul 2003, Published online: 16 Aug 2006
 
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Abstract

A simple one pot method, involving sequential Knoevenagel condensation of Meldrum's acid with aromatic aldehydes, conjugate reduction of ylidene Meldrum's acid using sodium borohydride followed by alkylation, to prepare mixed dialkylated derivatives of Meldrum's acid is described.

Acknowledgment

One of the authors (UVD) thanks UGC, New Delhi, for financial assistance.

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