A Facile Synthesis of [Tetrahydrofuran‐³H] Terazosin

Judith A. Egan PerkinElmer Life and Analytical Sciences, Inc., 549 Albany St., Boston, Massachusetts, 02118, USA

Steven M. Souza PerkinElmer Life and Analytical Sciences, Inc., 549 Albany St., Boston, Massachusetts, 02118, USA

Crist N. Filer PerkinElmer Life and Analytical Sciences, Inc., 549 Albany St., Boston, Massachusetts, 02118, USACorrespondence[email protected]

Abstract

An efficient synthesis of [³H] terazosin at high specific activity from prazosin is described.

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Acknowledgments

We wish to thank Drs. Puliyur Srinivasan and Mahendra Suryan of PerkinElmer Life and Analytical Sciences for obtaining the various NMR and mass spectra, respectively, and Dr. Scot Pounds for assistance with the tritiation.

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A Facile Synthesis of [Tetrahydrofuran‐³H] Terazosin

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A Facile Synthesis of [Tetrahydrofuran‐3H] Terazosin

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A Facile Synthesis of [Tetrahydrofuran‐³H] Terazosin