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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 12
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Original Articles

Iodobenzene Diacetate Mediated Solid‐State Synthesis of Heterocyclyl‐1,3,4‐oxadiazoles

V. S. Rao Chemistry Group, Birla Institute of Technology and Science, Pilani, 333 031, Rajasthan, IndiaCorrespondence[email protected]
&
K. V. G. Chandra Sekhar Chemistry Group, Birla Institute of Technology and Science, Pilani, 333 031, Rajasthan, India
Pages 2153-2157 | Received 10 Feb 2004, Published online: 17 Aug 2006
 
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Abstract

A simple and efficient method has been developed for the oxidation of various heterocyclyl acylhydrazones 3 with iodobenzene diacetate (IBD) to heterocyclyl‐1,3,4‐oxadiazoles 4 in solid state. The reaction took place at room temperature within few minutes. The products were isolated by simple aqueous work-up in good yields.

Acknowledgment

We wish to thank the RSIC, CDRI, Lucknow, India for analytical and spectral data.

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