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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 23
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Original Articles

An Efficient and Selective Deprotecting Method for Methoxymethyl Ethers

Yungui Peng The School of Chemistry and Chemical Engineering, Southwest Normal University, Beibei, Chongqing, 400715, ChinaCorrespondence[email protected]
,
Changyun Ji The School of Chemistry and Chemical Engineering, Southwest Normal University, Beibei, Chongqing, 400715, China
,
Yingchun Chen Chengdu Institute of Organic Chemistry, Chinese Academy of Sciences, Chengdu, China
,
Chengzhi Huang The School of Chemistry and Chemical Engineering, Southwest Normal University, Beibei, Chongqing, 400715, China
&
Yaozhong Jiang Chengdu Institute of Organic Chemistry, Chinese Academy of Sciences, Chengdu, China
Pages 4325-4330 | Received 24 May 2004, Published online: 10 Jan 2011
 
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Abstract

Methoxymethyl ethers were selectively deprotected to the corresponding phenols in high yields by CBr4 and PPh3 in aprotic solvent (ClCH2CH2Cl) under slightly thermal reaction conditions.

Acknowledgments

We thank the Ministry of Education Foundation of China No. 2002 (27) and the Southwest Normal University Doctoral Fund for financial support of the study.

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