Microwave‐promoted One‐Pot Three‐Component Reaction to [60]Fulleropyrrolidine Derivatives

Jianming Zhang Department of Chemistry, School of Science, Shanghai University, Shanghai, China

Wen Yang Department of Chemistry, School of Science, Shanghai University, Shanghai, China

Ping He Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Science, Shanghai, 200032, China

Shizheng Zhu Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Science, Shanghai, 200032, ChinaCorrespondence[email protected]

Sheng Wang Department of Chemistry, School of Science, Shanghai University, Shanghai, China

Abstract

Under microwave irradiation and solvent‐free condition, one‐pot three‐component reaction of C₆₀, amino acid and aldehyde gave the corresponding [60]fulleropyrrolidine derivatives via dipolar [2 + 3] cycloaddition in moderate to good yields. Compared to the conventional thermal heating method, it provides a convenient and expeditious route to N‐unsubstituted fulleropyrrolidines.

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Acknowledgments

The authors thank the National Natural Science Foundation of China (NNSFC) (No. 20372077) and Innovation Foundation of Chinese Academy of Sciences for financial support.

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Microwave‐promoted One‐Pot Three‐Component Reaction to [60]Fulleropyrrolidine Derivatives

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Microwave‐promoted One‐Pot Three‐Component Reaction to [60]Fulleropyrrolidine Derivatives

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