Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 1
236
Views
6
CrossRef citations to date
0
Altmetric
Original Articles

Synthesis and Structure of a Novel Disulfide‐Containing Aniline

, , , , , , & show all
Pages 129-135 | Received 20 Aug 2004, Published online: 05 Aug 2006
 

Abstract

A novel disulfide‐containing aniline, 5,8‐dihydro‐1H,4H‐2,3,6,7‐tetrathia‐anthracen‐9‐ylamine (6) was synthesized. The structures of the target compound and the intermediates have been identified by 1H NMR, MS, IR, Raman and elemental analysis. In addition, the structure of 9‐Nitro‐5,8‐dihydro‐1H,4H‐2,3,6,7‐tetrathia‐anthracene (5) was determined by single X‐ray analysis.

AcknowleDgment

We gratefully acknowledge financial support by the National Natural Science Foundation of China (No. 29833090).

Notes

a 1H NMR(D2O) δ 7.63(s, 1H, ph‐H), 4.37(s, 4H, o‐ph‐CH2), 4.24(s, 4H, m‐ph‐CH2).

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.