Abstract
Synth. Commun. 2005, 35, 1011
Synthesis of Bis‐1,4‐Dihydropyridine Derivatives
Songlei Zhu,1,2 Shujang Tu,1 Yuan Gao,3 Chunbao Miao,1 Tuanjie Li,1 Xiaojing Zhang,1 Fang Fang,1 and Daqing Shi1
1Department of Chemistry, Xuzhou Normal University, Key Laboratory of Biotechnology on Medical Plant Jiangsu, Xuzhou, Jiangsu, China
2Department of Chemistry, Xuzhou Medical College, Xuzhou, Jiangsu, China
3Department of Chemistry, Shenzhen University, Shenzhen, Guangdong, China
A series of bis‐1,4‐dihydropyridine derivatives were synthesized by the reaction of p‐phenylenedialdehyde or m‐phenylenedialdehyde and active methylene compounds.
Abstract
Synth. Commun. 2005, 35, 1017
Synthesis of Ribavirin Analogues Containing Amino‐Acid Residues
Daliang Li, Hongli Bao, Qitao Tan, Dongmei Cai, and Tianpa You
Chemistry Department, University of Science & Technology of China, Hefei, China
Abstract
Synth. Commun. 2005, 35, 1027
One‐Pot Synthesis of Tetrahydro‐2‐Methylidenefurans
Fumi Okabe, Yoshinobu Tagawa, and Kenji Yamagata
Faculty of Pharmaceutical Sciences, Fukuoka University, Fukuoka, Japan
Abstract
Synth. Commun. 2005, 35, 1033
Cetyltrimethylammonium Dichromate: A Phase‐Transferring Oxidant
Sabita Patel, Minati Kuanar, Biswa B. Nayak, H. Banichul, and Bijay K. Mishra
Center of Studies in Surface Science and Technology, Department of Chemistry, Sambalpur University, Jyoti Vihar, 768019, India
Abstract
Synth. Commun. 2005, 35, 1039
Mild and Solvent‐Free Alkynylation of Ketones on the KF/Alumina Surface
A. Sharifi, M. Mirzaei, and M. Reza Naimi‐Jamal
Chemistry & Chemical Engineering Research Center of Iran, Tehran, Iran
Solvent‐free alkynylation of diverse ketones on the surface of KF/alumina under mild conditions is described.
Abstract
Synth. Commun. 2005, 35, 1045
Aldol Condensations Catalyzed by PEG400 and Anhydrous K2CO3 without Solvent
Yu‐Qing Cao,1 Zhi Dai,1 Rui Zhang2, and Bao‐Hua Chen2
1College of Chemistry and Environmental Science, Hebei University, Hebei, P. R. China
2Hebei Changtian pharma Baoding, P. R. China
Aldol condensations of aromatic aldehydes with ketones under solvent‐free conditions to synthesize α,α′‐unsaturated ketones in good to excellent yields using PEG400 and powdered anhydrous K2CO3 as catalysts at 90 °C and 120 °C are described.
Abstract
Synth. Commun. 2005, 35, 1051
Fe3+‐Montmorillonite as Effective, Recyclable Catalyst for Paal–Knorr Pyrrole Synthesis under mild Conditions
Guoyong Song,1 Bo Wang,1 Guang Wang,2 Yuru Kang,1 Tao Yang,1 and Liming Yang1
1State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, China
2Key Laboratory of Gas Geochemistry, Lanzhou Institute of Geology, Chinese Academy of Sciences, Lanzhou, China
Fe3+‐montmorillonite clay catalyst was used for the first time for pyrroles preparation by Paal–Knorr condensation under mild conditions.
Abstract
Synth. Commun. 2005, 35, 1059
Catalysis of the Reaction of Cholesteryl Acetate with 4‐Phenyl‐1,2,4‐triazoline‐3,5‐dione by Lithium Perchlorate
W.J. Kinart,1 R.B. Nazarski,1 C.M. Kinart,2 Q.T. Thuong,1 and R. Oszczęda1
1Department of Organic Chemistry, University of Łódź, Narutowicza, Łódź, Poland
2Faculty of Physics and Chemistry, University of Łódź, Pomorska, Łódź, Poland
Abstract
Synth. Commun. 2005, 35, 1067
Synthesis of New Ferrocenyl‐Substituted Aziridines via the Gabriel–Cromwell Reaction
Özdemir Doğan,1 Serhat Zeytinci,1 and Adnan Bulut2
1Department of Chemistry, Middle East Technical University, Ankara, Turkey
2Department of Chemistry, Kırıkkale University, Kırıkkale, Turkey
Acryloyl‐ and crotonoylferrocenes are successfully converted to their corresponding aziridines by the Gabriel–Cromwell reaction in good yields.
Abstract
Synth. Commun. 2005, 35, 1077
Reaction of Active Methylene Groups with 1,2‐Di(BromoSeleno)Benzene toward Benzo‐1,3(2H)‐Diselenoles
Piotr Potaczek, Krystian Kloc, and Jacek Młochowski
Institute of Organic Chemistry, Biochemistry and Biotechnology, Wrocław University of Technology, Wyb. Wyspiańskiego, Wrocław, Poland
The tandem diselenylation of the active methylene compounds (2) with 1,2‐di(bromoseleno)benzene (1) toward 1,3(2H)diselenoes (3) is described.
Abstract
Synth. Commun. 2005, 35, 1085
Efficient Synthesis of Orthogonally Protected Spermidine and Norspermidine Derivatives
Ryszard Andruszkiewicz, Michał Radowski, and Zbigniew Czajgucki
Department of Pharmaceutical Technology and Biochemistry, Gdańsk University of Technology, Gdańsk, Poland
Orthogonally protected spermidine and norspermidine derivatives have been synthesized.
Abstract
Synth. Commun. 2005, 35, 1095
Synthesis of 1‐[(2‐Hydroxyethoxy)Methyl]‐6‐(5,6,7,8‐Tetrahydronaphthylmethyl‐1)Thymine as Novel Inhibitor against Drug‐Resistant HIV Mutants
Ge Meng, Yun‐Yan Kuang, Lei Ji, and Fen‐Er Chen
Department of Chemistry, Fudan University, Shanghai, China
Synthesis of two new 1‐[(2‐hydroxyethoxy)methyl]‐6‐(5,6,7,8‐tetrahydronaphthylmethyl‐1)thymine derivatives 10a–b, as potent inhibitors against a mutant type of HIV, starting from thymine, is described.
Abstract
Synth. Commun. 2005, 35, 1103
Oxidation of Aldehydes and Ketones into Carboxylic Acids and Esters Using 4‐Amino‐2‐Chloroperbenzoic Acid Supported on Silica Gel
Mohammed M. Hashemi,1 Dadkhoda Ghazanfari,2 Yousef Ahmadibeni,1 Zahed Karimi‐Jaberi,1 and Ali Ezabadi2
1Department of Chemistry, Sharif University of Technology, Tehran, Iran
2Department of Chemistry, Science and Research Branch, Islamic Azad University, Tehran, Iran
4‐Amino‐2‐chloroperbenzoic acid supported on silica gel was found to be a versatile and efficient oxidant for the oxidation of aldehydes and ketones to the corresponding carboxylic acids and esters.
Abstract
Synth. Commun. 2005, 35, 1109
Synthesis of N‐(4‐Methyl‐1,2,3,4‐Tetrahydro‐2 Quinolinyl)‐N‐Aryl Amines
Farideh Piri,1 Hojat Allah Zalfard,2 Agdas Gahramani,2 and Issa Yavari3
1Iran Polymer and Petrochemical Institute
2Department of Chemistry, University of Zanjan, Zanjan, Iran
3Department of Chemistry Tarbiat Modarres, Tehran, Iran
N‐(4‐methyl‐1,2,3,4‐tetrahydro‐2quinolinyl)‐N‐aryl amines are produced in reaction of aryl amines with isobutyl vinyl ether in very mild condition.
Abstract
Synth. Commun. 2005, 35, 1115
Preparation of 1,5‐Fused Tetrazoles Under Solvent‐Free Conditions
Hossein Eshghi1 and Asadollah Hassankhani2
1Department of Chemistry, Ferdowsi University of Mashhad, Mashhad, Iran
2Department of Chemistry, Sistan & Baluchestan University, Zahedan, Iran
Abstract
Synth. Commun. 2005, 35, 1121
Reduction of Nitro‐Aryl Compounds with Zinc in the Presence of Poly[N‐(2‐aminoethyl)acrylamido]trimethylammonium Chloride as a Phase‐Transfer Catalyst
Hossen Mahdavi1 and Bahman Tamami2
1Chemistry Department, Tehran University, Tehran, Iran
2Chemistry Department, Shiraz University, Shiraz, Iran
The new polymeric phase‐transfer catalyst, poly[N‐(2‐aminoethyl)acrylamido]trimethylammonium chloride resin, catalyzes the reduction of nitroarenes to the corresponding aromatic amines with zinc powder in water and with high yields under mild conditions.
Abstract
Synth. Commun. 2005, 35, 1129
Regioselective Reduction of β‐Enaminoesters
Syed Raziullah Hussaini and Mark G. Moloney
Department of Chemistry, Chemical Research Laboratory, University of Oxford, Oxford, U.K.
Abstract
Synth. Commun. 2005, 35, 1135
Synthesis of 3,5‐Diphenyl‐1H‐ Pyrazoles
B.A. Bhat,1 S.C. Puri,1 M.A. Qurishi,2 K.L. Dhar,1 and G.N. Qazi1
1Division of Natural Products Chemistry, Regional Research Laboratory (CSIR), Jammu, India
2Department of Chemistry, University of Kashmir, Srinagar, India
An efficient and convenient synthesis of 3,5‐diphenyl‐1H‐pyrazoles from chalcones by the action of hydrazine hydrate on chalcone‐epoxide followed by simultaneous dehydration is reported.