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A very high‐yielding reaction of bis(o‐nitrophenyl) carbonate with aliphatic amines under mild conditions has been developed. The resulting o‐nitrophenyl carbamates were characterized by IR, 1H‐NMR, 13C‐NMR, and elemental analysis.
M.S., C.C., M.T.C., and M.C.T. thank CNCSIS for financial support (Grant A, Cod CNCSIS 475/18/2000).
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