SYNTHESIS AND CHARACTERIZATION OF ORGANOTIN(IV) COMPLEXES OF N-(2-MERCAPTOPHENYL)-SALICYLALDIMINE

Laijin Tian Department of Chemistry, Zhejiang University, Hangzhou, 310027, People's Republic of China; Department of Chemistry, Qufu Normal University, Qufu, Shandong, 273165, People's Republic of China

Bin Zhao Department of Chemistry, Qufu Normal University, Qufu, Shandong, 273165, People's Republic of China

Qingsen Yu Department of Chemistry, Zhejiang University, Hangzhou, 310027, People's Republic of China

Zhicai Shang1 Department of Chemistry, Zhejiang University, Hangzhou, 310027, People's Republic of China

ABSTRACT

The organotin(IV) complexes of N-(2-mercaptophenyl)salicylaldimine,ROCOCH₂CH₂SnClL(L=OC₆H₄CH˭NC₆H₄S, R=alkyl), were synthesized by the reaction of 2-alkoxy carbonylethyltin trichlorides with N-(2-mercaptophenyl)salicylaldimine (H₂L) in the presence of triethylamine and were characterized by elemental analyses, IR, ¹H NMR spectra and X-ray single crystal diffraction. The structural features of these compounds are discussed.

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SYNTHESIS AND CHARACTERIZATION OF ORGANOTIN(IV) COMPLEXES OF N-(2-MERCAPTOPHENYL)-SALICYLALDIMINE

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SYNTHESIS AND CHARACTERIZATION OF ORGANOTIN(IV) COMPLEXES OF N-(2-MERCAPTOPHENYL)-SALICYLALDIMINE

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