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Advances in Applied Ceramics
Structural, Functional and Bioceramics
Volume 113, 2014 - Issue 4
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Original Articles

Characterisation and photocatalytic activity of SnO2 films via plasma electrolytic oxidation

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Pages 228-233 | Received 17 Nov 2013, Accepted 26 Jan 2014, Published online: 13 Feb 2014
 

Abstract

SnO2 films were prepared by plasma electrolytic oxidation technology in solution containing different concentrations. The structure and photocatalytic activity of the films were characterised by X-ray diffraction, SEM, EDX, Brunauer–Emmett–Teller (BET) and UV-vis spectrophotometer. The result shows that films consisted of pure SnO2, but the grain size increased with the increase of concentration. Porous and rough SnO2 films were formed on the substrate. The BET surface area increased with the increase of concentration and reached its maximum when the concentration of was 0·05M. The absorption edge of the films shifted from 370 to 408 nm when the concentration of increased from 0·01 to 0·03M. Degradation of rhodamine indicated that photocatalytic activity of film formed in 0·03M was highest due to its smaller grain, larger BET surface area and greater photon absorption.

Acknowledgement

The authors would gratefully acknowledge analytical and testing center of Huazhong University of Science and Technology for the tasks of test.

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