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Free Radical Research Communications Volume 16, 1992 - Issue 1
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Original Article

Mass Spectrometric Identification of the Radical Adducts of a Fluorescamine-Derivatized Nitroxide

David J. Kieber Department of Chemistry, Woods Hole Oceanographic Institution, Woods Hole, Massachusetts, 02543, USA; State University of New York, College of Environmental Science and Forestry, Chemistry Department, 1 Forestry Drive, Syracuse, NY, 13210, USA
,
Carl G. Johnson Department of Chemistry, Woods Hole Oceanographic Institution, Woods Hole, Massachusetts, 02543, USA
&
Neil V. Blough Department of Chemistry, Woods Hole Oceanographic Institution, Woods Hole, Massachusetts, 02543, USA
Pages 35-39 | Received 29 Apr 1991, Accepted 28 Oct 1991, Published online: 07 Jul 2009
 
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Abstract

The radical adducts of fluorescamine-derivatized 3-aminomethyl-2,2,5,5-tetrarnethyl-1-pyrrolidinyloxy free radical are readily identified by mass spectrometry employing a solid source probe and electron impact ionization.

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