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Original Articles

Micro-scale Synthesis and In-Situ Spectroscopic Characterization of Some Chemical Weapons Related Organophosphonate Compounds

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Pages 1429-1444 | Received 01 Jul 1997, Accepted 16 Feb 1998, Published online: 19 Aug 2006

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ArvindK. Gupta, DevendraK. Dubey & M.P. Kaushik. (2008) Dichlorodimethyl Hydantoin: An Efficient Reagent for One-Pot Synthesis of CWC-Related O,O-dialkyl, N,N-dialkyl Phosphoramidates. Phosphorus, Sulfur, and Silicon and the Related Elements 183:7, pages 1641-1658.
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DavidJ. McGarvey, JohnR. Stuff, BarryR. Williams & H. Dupont Durst. (2000) Vapor-Phase Infrared Spectral Study of Analogs of the Nerve Agent Sarin. Spectroscopy Letters 33:6, pages 795-819.
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Articles from other publishers (24)

Maciej Boczkowski, Stanisław Popiel & Jakub Nawała. (2024) Application of Chemical Ionization in the Analysis of Ethylphosphonic Acid Derivatives. Journal of the American Society for Mass Spectrometry 35:4, pages 714-727.
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I. V. Rybal’chenko, T. M. Baigil’diev & I. A. Rodin. (2021) Chromatography–Mass Spectrometry Analysis for the Determination of the Markers and Biomarkers of Chemical Warfare Agents. Journal of Analytical Chemistry 76:1, pages 26-40.
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Todd M. Alam & Charles J. Pearce. (2015) Infrared signature of micro-hydration in the organophosphate Sarin: an ab initio study. Journal of Molecular Modeling 21:7.
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Prabhat Garg, Ajay Purohit, Vijay K. Tak, Ajeet Kumar & D.K. Dubey. (2012) Liquid–liquid–solid microextraction and detection of nerve agent simulants by on-membrane Fourier transform infrared spectroscopy. Analytica Chimica Acta 751, pages 71-78.
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Adam J. Mott & Peter Rez. (2012) Calculated infrared spectra of nerve agents and simulants. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 91, pages 256-260.
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Deepak Pardasani, Vijay Tak, Ajay K. Purohit, Pankaj K. Kanaujia & Devendra K. Dubey. (2011) Gas Chromatography—Electron Ionization—Mass Spectrometry Analysis of O,O ′-Dialkyl Methylphosphonites for Verification Analysis of the Chemical Weapons Convention . European Journal of Mass Spectrometry 17:1, pages 57-64.
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Prabhat Garg, Deepak Pardasani, Avik Mazumder, Ajay Purohit & D. K. Dubey. (2010) Dispersive solid-phase extraction for in-sorbent Fourier-transform infrared detection and identification of nerve agent simulants in analysis for verification of chemical weapon convention. Analytical and Bioanalytical Chemistry 399:2, pages 955-963.
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Deepak Pardasani, Ajay Purohit, Avik Mazumder & D. K. Dubey. (2010) Gas chromatography-mass spectrometric analysis of trimethylsilyl derivatives of toxic hydrolyzed products of nerve agent VX and its analogues for verification of Chemical Weapons Convention. Analytical Methods 2:6, pages 661.
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Prabhat Garg, Ajay Purohit, Vijay K. Tak & D.K. Dubey. (2009) Enhanced detectability of fluorinated derivatives of N,N-dialkylamino alcohols and precursors of nitrogen mustards by gas chromatography coupled to Fourier transform infrared spectroscopy analysis for verification of chemical weapons convention. Journal of Chromatography A 1216:45, pages 7906-7914.
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Deepak Pardasani, Pankaj K. Kanaujia, Vijay Tak, Prabhat Garg, Avik Mazumder & Devendra K. Dubey. (2009) Gas Chromatography Electron Ionization Mass Spectrometric Analysis of O -Alkyl Methylphosphinates for Verification of Chemical Weapons Convention . European Journal of Mass Spectrometry 15:5, pages 579-585.
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Rajesh Kumar, Devendra K. Dubey, Arvind K. Gupta & M.P. Kaushik. (2008) Surface Mediated Synthesis of Unsymmetrical O,O -dialkyl Alkyl Pyrophosphonates using Neutral Alumina: Potential Chemical Weapons Convention Related Compounds . Journal of Chemical Research 2008:5, pages 273-277.
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Rajesh Kumar, Deepak Pardasani, Avik Mazumder, Devendra K. Dubey & Arvind K. Gupta. (2008) Microwave Induced Synthesis of O,O-Dialkyl Dialkylpyrophosphonates under Solvent Free Conditions: Markers of Nerve Agents. Australian Journal of Chemistry 61:6, pages 476.
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Paul A. D’Agostino. 2008. Forensic Science. Forensic Science 839 872 .
Arvinda K. Gupta, Deepak Pardasani, Pankaj K. Kanaujia, Vijay Tak & Devendra K. Dubey. (2006) Gas chromatography/mass spectrometric analysis of N , N ‐dialkylaminoethyl‐2‐chlorides and trimethylsilyl derivatives of N , N ‐dialkylaminoethan‐2‐ols for verification of the Chemical Weapons Convention . Rapid Communications in Mass Spectrometry 20:14, pages 2115-2119.
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Deepak Pardasani, Arvinda K. Gupta, Meehir Palit, Purushottam Shakya, Pankaj K. Kanaujia, K. Sekhar & Devendra K. Dubey. (2005) Gas chromatography/mass spectrometric analysis of methyl esters of N,N ‐dialkylaminoethane‐2‐sulfonic acids for verification of the Chemical Weapons Convention . Rapid Communications in Mass Spectrometry 19:21, pages 3015-3020.
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D. K. Dubey, Meehir Palit, A. K. Gupta, Deepak Pardasani, Purushottam Shakya & R. K. Srivastava. (2005) Study of electron ionization mass spectra of bis(trimethylsilyl) esters of alkylphosphonic and alkylthiophosphonic acids. Rapid Communications in Mass Spectrometry 19:12, pages 1763-1766.
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Arvind. K. Gupta, Meehir Palit, Deepak Pardasani, Purushottam Shakya, Rajendra K. Srivastava & Devendra K. Dubey. (2017) Micro-Synthesis and Electron Ionization Mass Spectral Analysis of O -Alkyl N,N -Dialkylphosphoramidocyanidates . European Journal of Mass Spectrometry 11:3, pages 309-318.
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Arvind K. Gupta, Purushottam D. Shakya, Deepak Pardasani, Meehir Palit & Devendra K. Dubey. (2005) Mass spectral analysis of synthones of nerve agents for verification of the Chemical Weapons Convention. Rapid Communications in Mass Spectrometry 19:8, pages 975-983.
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Meehir Palit, Deepak Pardasani, A. K. Gupta, Purushottam Shakya & D. K. Dubey. (2004) Microsynthesis and electron ionisation mass spectrometric analysis of chemical weapons convention (CWC)-related O,O-dialkyl-N,N-dialkylphosphoramidates. Analytical and Bioanalytical Chemistry 381:2, pages 477-486.
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Edwin W.J Hooijschuur, Charles E Kientz & Udo A.Th Brinkman. (2002) Analytical separation techniques for the determination of chemical warfare agents. Journal of Chromatography A 982:2, pages 177-200.
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Martin T. Söderström. 2007. Encyclopedia of Analytical Chemistry. Encyclopedia of Analytical Chemistry.
Mark D Brickhouse,William R Creasy, Barry R Williams, Kevin M Morrissey, Richard J O’Connor & H Dupont Durst. (2000) Multiple-technique analytical characterization of a mixture containing chemical-weapons simulant from a munition. Journal of Chromatography A 883:1-2, pages 185-198.
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Olli Kostiainen. 2000. Forensic Science. Forensic Science 405 435 .
John R. Stuff, William R. Creasy, Alex A. Rodriguez & H. Dupont Durst. (1999) Gas chromatography with atomic emission detection as an aid in the identification of chemical warfare related material. Journal of Microcolumn Separations 11:9, pages 644-651.
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