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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 6
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Original Articles

Efficient Synthesis of 1-(4′-Methylbenzoyl)- 3,3-Diethylthiourea Under Microwave Irradiation Using Potassium Fluoride on Alumina

H. Márquez Laboratorio de Síntesis Orgánica, Facultad de Química, Universidad de La Habana, Zona Postal 10400, Ciudad de La Habana, Cuba E-mail: [email protected]
,
A. Plutín Laboratorio de Síntesis Orgánica, Facultad de Química, Universidad de La Habana, Zona Postal 10400, Ciudad de La Habana, Cuba E-mail: [email protected]
,
Y. Rodríguez Laboratorio de Síntesis Orgánica, Facultad de Química, Universidad de La Habana, Zona Postal 10400, Ciudad de La Habana, Cuba E-mail: [email protected]
,
E. Perez Laboratorio de Síntesis Orgánica, Facultad de Química, Universidad de La Habana, Zona Postal 10400, Ciudad de La Habana, Cuba E-mail: [email protected]
&
A. Loupy Laboratoire des Réactions Sélectives sur Supports, ICMO, UMR 8615, building 410, Université Paris-Sud, 91405, Orsay-Cédex, France E-mail: [email protected]
Pages 1067-1073 | Received 24 Feb 1999, Published online: 04 Dec 2007

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Aamer Saeed, Ulrich Flörke & Mauricio F. Erben. (2014) A review on the chemistry, coordination, structure and biological properties of 1-(acyl/aroyl)-3-(substituted) thioureas. Journal of Sulfur Chemistry 35:3, pages 318-355.
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P. Singh, K. Natani, S. Jain, K. Arya & A. Dandia. (2006) Microwave-assisted rapid cyclization of lapachol, a main constituent of Heterophragma adenophyllum . Natural Product Research 20:2, pages 207-212.
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E.R. Pérez, N.C. Carnevalli, P.J. Cordeiro, U.P. Rodrigues-Filho & D.W. Franco. (2001) EFFICIENT SOLVENT-FREE MICROWAVE-ASSISTED ESTERIFICATION OF FUSEL OIL USING p-TsOH AND H3PW12O40 AS CATALYSTS. Organic Preparations and Procedures International 33:4, pages 395-400.
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Xiao-Dong Yang, Xiang-Hui Zeng, Yuan-Hong Zhao, Xue-Quan Wang, Zhi-Qiang Pan, Liang Li & Hong-Bin Zhang. (2010) Silica Gel-Mediated Amide Bond Formation: An Environmentally Benign Method for Liquid-Phase Synthesis and Cytotoxic Activities of Amides. Journal of Combinatorial Chemistry 12:3, pages 307-310.
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Anshu Dandia, Ruby Singh & Sumit Bhaskaran. (2010) Ultrasound promoted greener synthesis of spiro[indole-3,5′-[1,3]oxathiolanes in water. Ultrasonics Sonochemistry 17:2, pages 399-402.
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Anshu Dandia, Ruby Singh, Pritima Sarawgi & Sarita Khaturia. (2006) Multicomponent One-pot Diastereoselective Synthesis of Biologically Important Scaffold under Microwaves. Chinese Journal of Chemistry 24:7, pages 950-954.
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Heiddy Marquez, André Loupy, Osmar Calderon & Eduardo R. Pérez. (2006) An eco-friendly protocol for synthesis of thiourea derivatives: 1-benzoyl-3-benzylguanidine and 1-benzoyl-3-benzyl-O-ethylisourea. A possible non-purely thermal microwave assisted reaction. Tetrahedron 62:11, pages 2616-2621.
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Christian A.G.N. Montalbetti & Virginie Falque. (2005) Amide bond formation and peptide coupling. Tetrahedron 61:46, pages 10827-10852.
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Aleksandra Burczyk, André Loupy, Dariusz Bogdal & Alain Petit. (2005) Improvement in the synthesis of metallophthalocyanines using microwave irradiation. Tetrahedron 61:1, pages 179-188.
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Anshu Dandia, Kapil Arya, Meha Sati & Sangeeta Gautam. (2004) Microwave assisted green chemical synthesis of novel spiro[indole-pyrido thiazines]: a system reluctant to be formed under thermal conditions. Tetrahedron 60:24, pages 5253-5258.
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Benjamin E. Blass. (2002) KF/Al2O3 Mediated organic synthesis. Tetrahedron 58:46, pages 9301-9320.
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Satoshi Horikoshi, Hisao Hidaka & Nick Serpone. (2002) Environmental Remediation by an Integrated Microwave/UV-Illumination Method. 1. Microwave-Assisted Degradation of Rhodamine-B Dye in Aqueous TiO 2 Dispersions . Environmental Science & Technology 36:6, pages 1357-1366.
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Laurence Perreux, André Loupy & François Volatron. (2002) Solvent-free preparation of amides from acids and primary amines under microwave irradiation. Tetrahedron 58:11, pages 2155-2162.
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Pelle Lidström, Jason Tierney, Bernard Wathey & Jacob Westman. (2001) Microwave assisted organic synthesis—a review. Tetrahedron 57:45, pages 9225-9283.
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H. Marquez, A. Plutin, Y. Rodriguez, E. Perez & A. Loupy. (2010) ChemInform Abstract: Efficient Synthesis of 1‐(4′‐Methylbenzoyl)‐3,3‐diethylthiourea under Microwave Irradiation Using Potassium Fluoride on Alumina.. ChemInform 31:27.
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