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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 3
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Original Articles

Preparation of Primary Thioamides From Nitriles Using Sodium Hydrogen Sulfide and Diethylamine Hydrochloride

Mark L. Boys Department of Chemistry, Pfizer Global R&D, Ann Arbor, Michigan, USACorrespondence[email protected]
&
Victoria L. Downs Department of Chemistry, Pfizer Global R&D, Ann Arbor, Michigan, USA
Pages 295-298 | Received 28 Jul 2005, Published online: 19 Aug 2006

Citations (14)

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Read on this site (2)

Mauricio Acelas, Andrés Felipe Sierra & César A. Sierra. (2020) Exploring the nitro group reduction in low-solubility oligo-phenylenevinylene systems: Rapid synthesis of amino derivatives. Synthetic Communications 50:9, pages 1335-1352.
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Mátyás Milen, Péter Ábrányi-Balogh, András Dancsó & György Keglevich. (2012) Microwave-assisted synthesis of thioamides with elemental sulfur. Journal of Sulfur Chemistry 33:1, pages 33-41.
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Articles from other publishers (12)

Asger M. Koue, Fernando Montero, Lars M. Skjolding, Sergey Kucheryavskiy, Marco Maschietti & Christian M. Pedersen. (2024) Multifunctional biomass-based chemicals: H 2 S scavenging . Green Chemistry 26:4, pages 1984-1989.
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Yogesh Ashok Tayade, Yogesh Baburav Wagh & Dipak Sharadrao Dalal. (2023) β-cyclodextrin Mediated Green Synthesis of Bioactive Heterocycles. Current Organic Chemistry 27:12, pages 1036-1052.
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Ling Peng, Li Ma, Ying Ran, Yunfeng Chen & Zhigang Zeng. (2021) Metal-free three-component synthesis of thioamides from β-nitrostyrenes, amines and elemental sulfur. Tetrahedron Letters 74, pages 153092.
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Le Anh Nguyen, Quoc Anh Ngo, Pascal Retailleau & Thanh Binh Nguyen. (2021) Break‐and‐Build Strategy for the Synthesis of 2‐Benzoylbenzoxazoles from o ‐Aminophenols and Acetophenones . Advanced Synthesis & Catalysis 363:8, pages 2098-2103.
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Ewelina Zaorska, Tomasz Hutsch, Marta Gawryś-Kopczyńska, Ryszard Ostaszewski, Marcin Ufnal & Dominik Koszelewski. (2019) Evaluation of thioamides, thiolactams and thioureas as hydrogen sulfide (H2S) donors for lowering blood pressure. Bioorganic Chemistry 88, pages 102941.
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Yogesh A. Tayade, Asha D. Jangale & Dipak S. Dalal. (2018) Simple and Highly Efficient Synthesis of Thioamide Derivatives Using β‐Cyclodextrin as Supramolecular Catalyst in Water. ChemistrySelect 3:31, pages 8895-8900.
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PengFei Zhang, XianTing Cao, HuiYong Yang & Hui Zheng. (2018) A Simple Method for Synthesis of Thioamides and Application in Synthesis of 1,2,4-Thiadiazoles. HETEROCYCLES 96:3, pages 509.
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Xian-Ting Cao, Li Qiao, Hui Zheng, Hui-Yong Yang & Peng-Fei Zhang. (2018) A efficient protocol for the synthesis of thioamides in [DBUH][OAc] at room temperature. RSC Advances 8:1, pages 170-175.
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Tamashree Ghosh, Anshupriya Si & Anup Kumar Misra. (2017) Facile Transformation of Nitriles into Thioamides: Application to C ‐Glycosyl Nitrile Derivatives . ChemistrySelect 2:4, pages 1366-1369.
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Begur Vasanthkumar Varun, Ankush Sood & Kandikere Ramaiah Prabhu. (2014) A metal-free and a solvent-free synthesis of thio-amides and amides: an efficient Friedel–Crafts arylation of isothiocyanates and isocyanates. RSC Adv. 4:105, pages 60798-60807.
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Yanyang Qu, Zhengkai Li, Haifeng Xiang & Xiangge Zhou. (2013) Copper(II)‐Catalyzed Reactions of Dimethylformamide with Phenylacetonitrile and Sulfur to Form N,N ‐Dimethylthioamides . Advanced Synthesis & Catalysis 355:16, pages 3141-3146.
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Mark L. Boys & Victoria L. Downs. (2006) Preparation of Primary Thioamides from Nitriles Using Sodium Hydrogen Sulfide and Diethylamine Hydrochloride.. ChemInform 37:23.
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