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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 7
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Original Articles

Rapid, Acid‐Mediated Deprotection of Silyl Ethers Using Microwave Heating

R. David Crouch Department of Chemistry, Dickinson College, Carlisle, Pennsylvania, USACorrespondence[email protected]
&
Anna B. Williams Department of Chemistry, Dickinson College, Carlisle, Pennsylvania, USA
Pages 959-964 | Received 12 Oct 2005, Published online: 16 Aug 2006

Citations (8)

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Read on this site (2)

Amin Rostami, Firoz Ahmad-Jangi, Mohammad Rezgar Zarebin & Jamal Akradi. (2010) Green and Efficient Procedure for the Trimethylsilylation of Hydroxy Groups and Their Regeneration Using Sulfamic Acid as Recyclable Catalyst. Synthetic Communications 40:10, pages 1500-1507.
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Ardeshir Khazaei, Amin Rostami & Fatemeh Mantashlo. (2009) p-Toluenesulfonyl Chloride (p-TsCl)-Catalyzed Trimethylsilylation of Hydroxyl Groups Using Hexamethyldisilazane and Their Regeneration Under Mild Conditions: The First Example for Catalytic Application of p-Toluenesulfonyl Chloride. Phosphorus, Sulfur, and Silicon and the Related Elements 184:9, pages 2288-2296.
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Articles from other publishers (6)

Claudia Pasqualini, Federica Poggialini, Chiara Vagaggini, Annalaura Brai & Elena Dreassi. (2022) A Greener Technique for Microwave-Assisted O-Silylation and Silyl Ether Deprotection of Uridine and Other Substrates. Chemistry 4:4, pages 1714-1722.
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William D. G. Brittain & Steven L. Cobb. (2019) Tetrafluoropyridyl (TFP): a general phenol protecting group readily cleaved under mild conditions. Organic & Biomolecular Chemistry 17:8, pages 2110-2115.
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. 2014. Greene's Protective Groups in Organic Synthesis. Greene's Protective Groups in Organic Synthesis 17 471 .
R. David Crouch. (2013) Selective deprotection of silyl ethers. Tetrahedron 69:11, pages 2383-2417.
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Syed Tasadaque A. Shah, Surendra Singh & Patrick J. Guiry. (2009) A Novel, Chemoselective and Efficient Microwave-Assisted Deprotection of Silyl Ethers with Selectfluor. The Journal of Organic Chemistry 74:5, pages 2179-2182.
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R. David Crouch & Anna B. Williams. (2006) Rapid, Acid‐Mediated Deprotection of Silyl Ethers Using Microwave Heating.. ChemInform 37:35.
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