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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 8
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Original Articles

New Procedure for One‐Pot Synthesis of 3,4‐Dihydropyrimidin‐2(1H)‐ones by Biginelli Reaction

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Pages 1299-1310 | Received 16 Aug 2007, Published online: 17 Apr 2008

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Heshmatollah Alinezhad & Khatereh Pakzad. (2020) Green Synthesis of Copper Oxide Nanoparticles with an Extract of Euphorbia maculata and Their Use in the Biginelli Reaction. Organic Preparations and Procedures International 52:4, pages 319-327.
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AbdolR. Hajipour & Mohadeseh Seddighi. (2012) Pyridinium-Based Brønsted Acidic Ionic Liquid as a Highly Efficient Catalyst for One-Pot Synthesis of Dihydropyrimidinones. Synthetic Communications 42:2, pages 227-235.
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Jianzhou Gui, Dan Liu, Chan Wang, Feng Lu, Jingzhao Lian, Heng Jiang & Zhaolin Sun. (2009) One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones Catalyzed by Acidic Ionic Liquids Under Solvent-Free Conditions. Synthetic Communications 39:19, pages 3436-3443.
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Articles from other publishers (24)

Ryohei Kakuchi, Kiho Matsubara, Jordan F. Madrid, Bin Jeremiah D. Barba, Masaaki Omichi, Yuji Ueki & Noriaki Seko. (2022) A-la-carte surface functionalization of organic materials via the combination of radiation-induced graft polymerization and multi-component reactions. MRS Communications 12:5, pages 552-564.
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Mohammad Ali Karimi Zarchi, Farhad Hajati & Bibi Fatemeh Mirjalili. (2022) A facile one-pot three component synthesis of 3, 4-dihydropyrimidin-2(1H)-ones or thiones promoted by a polymer-supported BF3 under solvent-free conditions. Research on Chemical Intermediates 48:8, pages 3449-3473.
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Samia Mammeri, Nadjib Chafai, Hassina Harkat, Rachida Kerkour & Salah Chafaa. (2021) Protection of Steel Against Corrosion in Acid Medium Using Dihydropyrimidinone Derivatives: Experimental and DFT Study. Iranian Journal of Science and Technology, Transactions A: Science 45:5, pages 1607-1619.
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Joana F. Campos & Sabine Berteina-Raboin. (2020) Greener Synthesis of Nitrogen-Containing Heterocycles in Water, PEG, and Bio-Based Solvents. Catalysts 10:4, pages 429.
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Aleksandra Kęciek, Daniel Paprocki, Dominik Koszelewski & Ryszard Ostaszewski. (2020) Evaluation of alcohols as substrates for the synthesis of 3,4-dihydropyrimidin-2(1H)-ones under environmentally friendly conditions. Catalysis Communications 135, pages 105887.
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Reşit Yıldız. (2018) Adsorption and inhibition effect of 2,4-diamino-6-hydroxypyrimidine for mild steel corrosion in HCl medium: experimental and theoretical investigation. Ionics 25:2, pages 859-870.
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Daniel Paprocki, Arleta Madej, Dominik Koszelewski, Anna Brodzka & Ryszard Ostaszewski. (2018) Multicomponent Reactions Accelerated by Aqueous Micelles. Frontiers in Chemistry 6.
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Robert Pawłowski, Ewelina Zaorska, Sebastian Staszko & Anna Szadkowska. (2018) Copper(I)-catalyzed multicomponent reactions in sustainable media. Applied Organometallic Chemistry 32:4, pages e4256.
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Muralidhar Allam, A. K. D. Bhavani & Sumathi Vodnala. (2017) The new green procedure for pyrazolopyrimidinone based dihydropyrimidinones and their antibacterial screening. Russian Journal of General Chemistry 87:11, pages 2712-2718.
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Abel Crespo, Abdelaziz El Maatougui, Jhonny Azuaje, Luz Escalante, María Majellaro, María Isabel Loza, José Brea, María Isabel Cadavid, Hugo Gutiérrez-de-Terán & Eddy Sotelo. (2017) Exploring the influence of the substituent at position 4 in a series of 3,4-dihydropyrimidin-2(1H)-one A2B adenosine receptor antagonists. Chemistry of Heterocyclic Compounds 53:3, pages 316-321.
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M. Hajjami & E. Ghiasbeygi. (2016) First catalyst- and solvent-free synthesis of 3,4-dihydropyrimidin-2(1H)-ones and -thiones. Russian Journal of Organic Chemistry 52:3, pages 429-432.
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Akbar Mobinikhaledi, Naser Foroughifar & Alireza Khajeh-Amiri. (2015) N-Propylcarbamothioyl benzamide complex of Bi(III) supported on superparamagnetic Fe3O4/SiO2 nanoparticles as a highly efficient and magnetically recoverable heterogeneous nanocatalyst for the one-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones/thiones (DHPMs) via the Biginelli reaction. Reaction Kinetics, Mechanisms and Catalysis 117:1, pages 59-75.
Crossref
Farhad Hatamjafari. (2014) An Efficient One-Pot Multi-Component Synthesis of 3,4-Dihydropyrimidin-2-(1H)-Ones/Thiones Catalyzed by Bismuth (III) Sulfate Trihydrate under Solvent-Free Conditions. Organic Chemistry International 2014, pages 1-5.
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Anamika Khaskel, Prasanta Gogoi, Pranjit Barman & Biman Bandyopadhyay. (2014) Grindstone chemistry: a highly efficient and green method for synthesis of 3,4-dihydropyrimidin-2-(1H)-ones by l -tyrosine as an organocatalyst: a combined experimental and DFT study . RSC Advances 4:67, pages 35559.
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Chandrabhan Verma, M.A. Quraishi & E.E. Ebenso. (2013) Thermodynamics and Electrochemical Investigation of (4-(2-amino-6-(cyclopropylamino)-9H-purin-9-yl) cyclopent-2-enyl) Methanol Sulphate as Green and Effective Corrosion Inhibitor for Mild Steel in 1M Hydrochloric Acid. International Journal of Electrochemical Science 8:11, pages 12238-12251.
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Eskandar Kolvari & Maryam Mirzaeeyan. (2013) Al(NO 3 ) 3  · 9H 2 O: An Efficient Catalyst for the One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1 H )-ones Both under Reflux or Solvent-Free Conditions . Journal of Chemistry 2013, pages 1-5.
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Jian Li, Xueli Xu, Kai Shi, Yong Zhou, Xian Luo & Yue Wu. (2012) Molecular Dynamics and Quantum Chemical Calculation for 3,4-Dihydropyrimidin-2(1H)-Ones As Corrosion Inhibitors of Mild Steel in 1M Hydrochloric Acid Solution. International Journal of Electrochemical Science 7:10, pages 9580-9591.
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Kawaljit Singh & Kamaljit Singh. 2012. 223 308 .
Santosh Takale, Sanket Parab, Kiran Phatangare, Rajaram Pisal & Atul Chaskar. (2011) IBX in aqueous medium: a green protocol for the Biginelli reaction. Catalysis Science & Technology 1:7, pages 1128.
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Dileep Kumar Yadav, B. Maiti & M.A. Quraishi. (2010) Electrochemical and quantum chemical studies of 3,4-dihydropyrimidin-2(1H)-ones as corrosion inhibitors for mild steel in hydrochloric acid solution. Corrosion Science 52:11, pages 3586-3598.
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A. Karamat, M. A. Khan & A. Sharif. (2010) Metal Acetate Mediated Biginelli One-Pot Synthesis. Journal of the Chinese Chemical Society 57:5A, pages 1099-1101.
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Yi Wang, Feng Xu, You-Ping Tian, Hui-Li Li & Jian-Jun Wang. (2009) CuX 2 (X = Cl, Br) as Catalysts for Pechmann Reaction: Synthesis of 4-substituted Coumarins . Journal of Chemical Research 2009:6, pages 339-341.
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Maksim A. Kolosov, Valeriy D. Orlov, Dmitriy A. Beloborodov & Victor V. Dotsenko. (2008) A chemical placebo: NaCl as an effective, cheapest, non-acidic and greener catalyst for Biginelli-type 3,4-dihydropyrimidin-2(1H)-ones (-thiones) synthesis. Molecular Diversity 13:1, pages 5-25.
Crossref
Feng Xu, Jian‐Jun Wang & You‐Ping Tian. (2008) ChemInform Abstract: New Procedure for One‐Pot Synthesis of 3,4‐Dihydropyrimidin‐2(1H)‐ones by Biginelli Reaction.. ChemInform 39:38.
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