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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 4
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Original Articles

Efficient, Solvent-Free, Microwave-Enhanced Condensation of 5,5-Dimethyl-1,3-cyclohexanedione with Aldehydes and Imines Using LiBr as Inexpensive, Mild Catalyst

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Pages 510-517 | Received 19 Jan 2009, Published online: 03 Feb 2010

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Soukaina Chehab, Youssef Merroun, Rachida Ghailane, Said Boukhris & Abdelaziz Souizi. (2023) Na2Ca(HPO4)2, an Efficient, Reusable Eco-Friendly Catalyst for the Synthesis of 1,8-Dioxo-Octahydroxanthenes and Biscoumarin Derivatives. Polycyclic Aromatic Compounds 43:6, pages 4906-4923.
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Divya Verma, Vikash Sharma, Shubha Jain & Gunadhor Singh Okram. (2020) Ultrasound-assisted synthesis of 1, 8-dioxodecahydroacridine derivatives in presence of Ag doped CdS nanocatalyst. Journal of Dispersion Science and Technology 41:8, pages 1145-1158.
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S. Sheik Mansoor, K. Aswin, K. Logaiya & S.P.N. Sudhan. (2014) Aqua-mediated synthesis of acridinediones with reusable silica-supported sulfuric acid as an efficient catalyst. Journal of Taibah University for Science 8:3, pages 265-275.
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Dhruva Kumar, Suresh & JagirS. Sandhu. (2013) Aldonitrones as Aldehyde Equivalents: An Efficient, Green, and Novel Protocol for the Synthesis of 1,8-Dioxo-octahydroxanthenes. Synthetic Communications 43:20, pages 2739-2747.
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Biswanath Das, J. Kashanna, Rathod Aravind Kumar & Paramesh Jangili. (2012) Efficient Organocatalytic Synthesis of 1,8-Dioxo-octahydroxanthenes. Synthetic Communications 42:19, pages 2876-2884.
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Sureshkumar Mahalingam, Ephraim Muriithi Kiarii, Thangaraj Thiruppathiraja, Arul Murugesan, Senthilkumar Lakshmipathi, Talent Raymond Makhanya & Robert M. Gengan. Microwave Hantzsch Synthesis of Quinolinyl-Dihydropyridines Supported by Cs-BNT Catalyst and DFT Investigations. Polycyclic Aromatic Compounds 0:0, pages 1-27.
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Fatemeh Sadat Hosseininasab & Hamid Reza Memarian. (2022) Efficient synthesis of decahydroacridine-1,8-diones and polyhydroquinolines using the step-wise method. Research on Chemical Intermediates 48:4, pages 1515-1540.
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M. E. Navgire, S. R. Bhitre, A. A. Yelwande & M. K. Lande. (2022) One-Pot Synthesis of 1,8-Dioxodecahydroacridines Catalyzed by Carbon-Doped MoO3. Russian Journal of Organic Chemistry 58:3, pages 394-404.
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Bitan Sardar, Ramen Jamatia, Debjyoti Pal & Dipankar Srimani. (2021) Multicomponent Dehydrogenative Synthesis of Acridine‐1,8‐diones Catalyzed by Ru‐doped Hydrotalcite. Asian Journal of Organic Chemistry 10:8, pages 2195-2204.
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G. Lavanya, K. Venkatapathy, C.J. Magesh, P.T. Perumal, R. Sathishkumar & P. Amudha. (2019) The First Recyclable, Nanocrystalline CdS Thin Film Mediated Eco‐benign Synthesis Of Hantzsch 1, 4 Dihyropyridines, 1, 8‐Dioxodecahydroacridine and Polyhydroquinolines derivatives. Applied Organometallic Chemistry 33:9.
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Sandeep S. Kahandal, Anand S. Burange, Sandip R. Kale, Pepijn Prinsen, Rafael Luque & Radha V. Jayaram. (2017) An efficient route to 1,8-dioxo-octahydroxanthenes and -decahydroacridines using a sulfated zirconia catalyst. Catalysis Communications 97, pages 138-145.
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R. Mirsafaei, S. Delzendeh & A. Abdolazimi. (2016) Synthesis and characterization of reusable nano-order SO3H-KIT-5 as a heterogeneous catalyst for eco-friendly synthesis of 1,4-dihydropyridines. International Journal of Environmental Science and Technology 13:9, pages 2219-2226.
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Masoud Nasr-Esfahani, Morteza Montazerozohori & Tooba Abdizadeh. (2015) Nanorod vanadatesulfuric acid (VSA NRs)-catalyzed green synthesis of hexahydroacridine-1,8-diones in solvent-free conditions. Comptes Rendus. Chimie 18:5, pages 547-553.
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Anne M. Reeve. (2014) Reaction of Dimedone and Benzaldehyde: A Discovery-Based Lab for Second-Semester Organic Chemistry. Journal of Chemical Education 92:3, pages 582-585.
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Ilangovan Pugazhenthi, Shaik Mohammed Ghouse, Fazlur-Rahman Nawaz Khan, Euh Duck Jeong, Jong Seong Bae, Jong-Pil Kim, Eun Hyuk Chung, Yadavalli Suneel Kumar & Changalraya Dasaradhan. (2015) Water mediated reactions: TiO 2 and ZnO nanoparticle catalyzed multi component domino reaction in the synthesis of tetrahydroacridinediones, acridindiones, xanthenones and xanthenes . RSC Advances 5:22, pages 17257-17268.
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Bubun Banerjee & Goutam Brahmachari. (2014) Ammonium Chloride Catalysed One-pot Multicomponent Synthesis of 1,8-dioxo-octahydroxanthenes and N -aryl-1,8-dioxodecahydroacridines Under Solvent Free Conditions . Journal of Chemical Research 38:12, pages 745-750.
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N. Tarannum & M. Singh. (2014) Facile eco-friendly synthesis of 3,4,6,7-tetrahydro-3,3,6,6-tetramethyl-2H-xanthene 1,8(5H,9H)-dione, crystal structure and theoretical study. Crystallography Reports 59:7, pages 987-992.
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Ghodsi Mohammadi Ziarani, Alireza Badiei, Malihe Hassanzadeh & Somayeh Mousavi. (2014) Synthesis of 1,8-dioxo-decahydroacridine derivatives using sulfonic acid functionalized silica (SiO2-Pr-SO3H) under solvent free conditions. Arabian Journal of Chemistry 7:3, pages 335-339.
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Shenghui Li, Shan Ding, Shengjie Xu, Jinchao Zhang, Shuxiang Wang, Chuanqi Zhou & Xiaoliu Li. (2013) Iodine-catalyzed three-component one-pot synthesis of novel 1,8-dioxo-decahydroacridines derivatives bearing benzene sulfonamide moiety. Research on Chemical Intermediates 40:5, pages 2091-2102.
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Yu-peng Liu, Jin-ming Liu, Xin Wang, Tie-ming Cheng & Run-tao Li. (2013) Multicomponent reactions leading to symmetric and asymmetric multi-substituted 1,4-dihydropyridines on montmorillonite. Tetrahedron 69:25, pages 5242-5247.
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Jing-Jing Xia & Ke-Hua Zhang. (2012) Synthesis of N-substituted Acridinediones and Polyhydroquinoline Derivatives in Refluxing Water. Molecules 17:5, pages 5339-5345.
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Bai Lin Li, Hua Ding Liang, Ai Guo Zhong & Dan Qian Xu. (2011) The Novel SO<sub>3</sub>H-Functionalized Ionic Liquids Promoted Synthesis of Xanthenedione Derivatives in Aqueous Media under Microwave Irradiation. Advanced Materials Research 391-392, pages 1354-1357.
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Kamalakar P. Nandre, Vijay S. Patil & Sidhanath V. Bhosale. (2011) CsF mediated rapid condensation of 1,3-cyclohexadione with aromatic aldehydes: Comparative study of conventional heating vs. ambient temperature. Chinese Chemical Letters 22:7, pages 777-780.
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Swapna Kokkirala, Narayana Murthy Sabbavarapu & Venkata Durga Nageswar Yadavalli. (2011) β-Cyclodextrin mediated synthesis of 1,8-dioxooctahydroxanthenes in water. European Journal of Chemistry 2:2, pages 272-275.
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P.P. Salvi, A.M. Mandhare, A.S. Sartape, D.K. Pawar, S.H. Han & S.S. Kolekar. (2011) Brønsted acidic ionic liquids promoted cyclocondensation reaction: Synthesis of 1,8-dioxo-octahydroxanthene. Comptes Rendus. Chimie 14:10, pages 883-886.
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Dhruva Kumar & Jagir S. Sandhu. (2010) ChemInform Abstract: Efficient, Solvent‐Free, Microwave‐Enhanced Condensation of 5,5‐Dimethyl‐1, 3‐Cyclohexanedione with Aldehydes and Imines Using LiBr as Inexpensive, Mild Catalyst.. ChemInform 41:31.
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