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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 13
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Original Articles

Rapid and Cheap Synthesis of Benzimidazoles via Intermittent Microwave Promotion: A Simple and Potential Industrial Application of Air as Oxidant

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Pages 1963-1977 | Received 05 Jun 2008, Published online: 08 Jun 2010

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Soumia Belkharchach, Hana Ighachane, Abdelali Rochdi, Mustapha Ait Ali & Hassan B. Lazrek. (2021) One-pot Synthesis of Benzimidazoles Using H2SO4@HTC as Catalyst. Organic Preparations and Procedures International 53:3, pages 268-277.
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Marzieh Haghverdi, Azadeh Tadjarodi, Naeimeh Bahri-laleh & Mahdi Nekoomanesh Haghighi. (2017) Cobalt complexes based on 2-(1H-benzimidazol-2-yl)-phenol derivatives: preparation, spectral studies, DFT calculations and catalytic behavior toward ethylene oligomerization. Journal of Coordination Chemistry 70:11, pages 1800-1814.
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Hui Han, Zhen‐Jiang Xu, Limin Wang & Jianwei Han. (2024) Manganese Catalyzed Oxidative Coupling of Aromatic Diamines and Alcohols with Aminoxyl Radicals in the Synthesis of Benzimidazoles. Asian Journal of Organic Chemistry.
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Zohor Mohammad Mahdi Alzhrani, Mohammad Mahboob Alam & Syed Nazreen. (2022) Recent Advancements on Benzimidazole: A Versatile Scaffold in Medicinal Chemistry. Mini-Reviews in Medicinal Chemistry 22:2, pages 365-386.
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Prashant B. Hiremath & Kantharaju Kamanna. (2021) Ultrasound-Promoted Sustainable Synthesis and Antimicrobial Evaluation of 2-Aryl Benzimidazoles Catalyzed by BPAE at Room Temperature. Current Organocatalysis 8:3, pages 338-352.
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Samiran HalderArup Datta. (2020) Highly Efficient Chemoselective Synthesis of 2-Aryl-1-arylmethyl-1H-Benzimidazoles by Using TiCp2Cl2 Catalyst. Oriental Journal Of Chemistry 36:6, pages 1173-1178.
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Sanju Das, Samrat Mallick & Suman De Sarkar. (2019) Cobalt-Catalyzed Sustainable Synthesis of Benzimidazoles by Redox-Economical Coupling of o -Nitroanilines and Alcohols . The Journal of Organic Chemistry 84:18, pages 12111-12119.
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Dao‐Qing Dong, Wen‐Jing Chen, Yun Yang, Xing Gao & Zu‐Li Wang. (2019) Merrifield Resin Supported Ionic Liquids/Iodide as an Efficient and Recyclable Catalyst for the Synthesis of Benzimidazoles. ChemistrySelect 4:8, pages 2480-2483.
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Yu-qin Jiang, Shu-hong Jia, Xi-yong Li, Ya-min Sun, Wei Li, Wei-wei Zhang & Gui-qing Xu. (2017) An efficient NaHSO3-promoted protocol for chemoselective synthesis of 2-substituted benzimidazoles in water. Chemical Papers 72:5, pages 1265-1276.
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Sami Sajjadifar, Zeinab Arzehgar & Azadeh Ghayuri. (2017) Zn 3 (BTC) 2 as a Highly Efficient Reusable Catalyst for the Synthesis of 2‐Aryl‐1 H ‐Benzimidazole . Journal of the Chinese Chemical Society 65:2, pages 205-211.
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Sunita Joshi, Santosh Kumari, Eduardo Chamorro, Debi D. Pant & Rajeev Sakhuja. (2016) Fluorescence Quenching of a Benzimidazolium–based Probe for Selective Detection of Picric Acid in Aqueous Medium. ChemistrySelect 1:8, pages 1756-1762.
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Jiatao Yu & Ming Lu. (2015) Iron-catalyzed highly efficient aerobic oxidative synthesis of benzimidazoles direct from oximes in water. Research on Chemical Intermediates 42:2, pages 471-479.
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Zhuohua Sun, Giovanni Bottari & Katalin Barta. (2015) Supercritical methanol as solvent and carbon source in the catalytic conversion of 1,2-diaminobenzenes and 2-nitroanilines to benzimidazoles. Green Chemistry 17:12, pages 5172-5181.
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Ye-Sol Lee, Yeon-Ho Cho, SeungJae Lee, Jong-Kwan Bin, JoongHwan Yang, GeeSung Chae & Cheol-Hong Cheon. (2015) Significant facilitation of metal-free aerobic oxidative cyclization of imines with water in synthesis of benzimidazoles. Tetrahedron 71:4, pages 532-538.
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Jin-Feng Xiong, Jian-Xiao Li, Guang-Zhen Mo, Jing-Pei Huo, Jin-Yan Liu, Xiao-Yun Chen & Zhao-Yang Wang. (2014) Benzimidazole Derivatives: Selective Fluorescent Chemosensors for the Picogram Detection of Picric Acid. The Journal of Organic Chemistry 79:23, pages 11619-11630.
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Meihong Jin, Guowei Song, Zhenjiang Li, Feng Zhou, Bo Fan & Pingkai Ouyang. (2014) Efficient Synthesis of 2‐Aryl‐1‐arylmethyl‐1 H ‐benzimidazoles in Ball Mill without Solvent . Journal of Heterocyclic Chemistry 51:6, pages 1838-1843.
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Pai Peng, Jin-Feng Xiong, Guang-Zhen Mo, Jia-Li Zheng, Ren-Hong Chen, Xiao-Yun Chen & Zhao-Yang Wang. (2014) A concise synthesis of benzimidazoles via the microwave-assisted one-pot batch reaction of amino acids up to a 10-g scale. Amino Acids 46:10, pages 2427-2433.
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Jiatao Yu, Yonggen Xia & Ming Lu. (2014) l ‐Proline: an efficient N,O‐bidentate ligand for copper‐catalyzed intramolecular cyclization reaction of 2‐iodoanilines with nitriles for the synthesis of benzimidazoles . Applied Organometallic Chemistry 28:10, pages 764-767.
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Sehyun Park, Jaehun Jung & Eun Jin Cho. (2014) Visible‐Light‐Promoted Synthesis of Benzimidazoles. European Journal of Organic Chemistry 2014:19, pages 4148-4154.
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Jiatao Yu & Ming Lu. (2014) [C 12 mim]Br: A Temperature‐dependent Phase Transfer Catalyst and Its Application for Aerobic Oxidative Synthesis of 2‐Aryl Benzimidazoles, Benzoxazoles or Benzothiozoles Catalyzed by TEMPO Based Ionic Liquid . Journal of the Chinese Chemical Society 61:5, pages 578-582.
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Guo-Yi Bai, Xing-Wang Lan, Guo-Feng Chen, Xiao-Fang Liu, Tian-Yu Li & Ling-Juan Shi. (2014) A novel sodium iodide and ammonium molybdate co-catalytic system for the efficient synthesis of 2-benzimidazoles using hydrogen peroxide under ultrasound irradiation. Ultrasonics Sonochemistry 21:2, pages 520-526.
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Yekkirala Venkateswarlu, Sudhagani Ramesh Kumar & Panuganti Leelavathi. (2013) Facile and efficient one-pot synthesis of benzimidazoles using lanthanum chloride. Organic and Medicinal Chemistry Letters 3:1.
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Jiatao Yu, Jian Xu & Ming Lu. (2013) Copper‐catalyzed highly efficient aerobic oxidative synthesis of benzimidazoles, benzoxazoles and benzothiazoles from aromatic alcohols under solvent‐free conditions in open air at room temperature. Applied Organometallic Chemistry 27:10, pages 606-610.
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Joanna V. Geden, Alpa K. Pancholi & Michael Shipman. (2013) Palladium-Catalyzed Multicomponent Synthesis of 2-Aryl-2-imidazolines from Aryl Halides and Diamines. The Journal of Organic Chemistry 78:8, pages 4158-4164.
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Xun Zhu & Yunyang Wei. (2019) An Efficient and Environmental Benign Synthesis of 2-benzimidazoles and 2-benzothiazoles Using CeCl 3 -NaI as Catalyst . Journal of Chemical Research 37:2, pages 119-121.
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Zhen-Ting Du, Dong Lu, Jia Wu, Liang-Zhu Huang, Bo-Lin Ma & Tao Zhang. (2013) Microwave-Assisted Syntehsis of 2-Substituted 1H-Benzo[d]imidazoles and Their Antifungal Activities in vitro. HETEROCYCLES 87:7, pages 1545.
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Hossein Eshghi, Mohammad Rahimizadeh, Ali Shiri & Parisa Sedaghat. (2012) One-pot Synthesis of Benzimidazoles and Benzothiazoles in the Presence of Fe(HSO 4 ) 3 as a New and Efficient Oxidant . Bulletin of the Korean Chemical Society 33:2, pages 515-518.
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Chenjie Zhu & Yunyang Wei. (2011) An Inorganic Iodine‐Catalyzed Oxidative System for the Synthesis of Benzimidazoles Using Hydrogen Peroxide under Ambient Conditions. ChemSusChem 4:8, pages 1082-1086.
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Xiu-Mei Song, Ning Wang, Zhao-Yang Wang & Zong-Cai Feng. (2011) 3-Chloro-4-dimethylamino-5-[(1 R ,2 S ,5 R )-2-isopropyl-5-methylcyclohexyloxy]furan-2(5 H )-one . Acta Crystallographica Section E Structure Reports Online 67:6, pages o1485-o1486.
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Larry Yet. 2011. 231 266 .
Zhengzhou Mao, Zhaoyang Wang, Jingning Li, Xiumei Song & Yufen Luo. (2010) ChemInform Abstract: Rapid and Cheap Synthesis of Benzimidazoles via Intermittent Microwave Promotion: A Simple and Potential Industrial Application of Air as Oxidant.. ChemInform 41:51.
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