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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 6
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Original Articles

FeCl3 Immobilized in Al-MCM 41: An Efficient Catalyst System for the Biginelli Reaction

Hossein A. Oskooie Department of Chemistry, School of Science, Alzahra University, Vanak, Tehran, Iran
,
Majid M. Heravi Department of Chemistry, School of Science, Alzahra University, Vanak, Tehran, IranCorrespondence[email protected]
,
Narges Karimi Department of Chemistry, School of Science, Alzahra University, Vanak, Tehran, Iran
&
Maryam H. Monjezy Department of Chemistry, School of Science, Alzahra University, Vanak, Tehran, Iran
Pages 826-831 | Received 22 Nov 2009, Published online: 25 Feb 2011

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Ali Rahmatpour & Ghazaleh Donyapeyma. (2022) Titanium tetrachloride immobilized on cross-linked poly(N-vinyl-2-pyrrolidone) as a recyclable heterogeneous catalyst for one-pot three component synthesis of 3, 4-dihydropyrimidin-2(1H)-ones/thiones. Synthetic Communications 52:5, pages 678-693.
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Articles from other publishers (28)

Selvi Arumugam, Nangan Senthilkumar, Natesan Thirumalaivasan, Govindaraj Dharman, Saravanan Pandiaraj, Mostafizur Rahaman, Manikandan Palaniappan, Rubiga Muthusami, Tamiliniyaa Manogaran, Lavanya Mari, Kuppusamy Kanagaraj, Rajakumar Govindasamy & Rajavel Rangappan. (2023) Heterogenous copper(II) schiff-base complex immobilized mesoporous silica catalyst for multicomponent biginelli reaction. Journal of Organometallic Chemistry 998, pages 122804.
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Nadia A. A. Elkanzi, Asmaa M. Kadry, Rasha M. Ryad, Rania B. Bakr, Mahmoud Abd El Aleem Ali Ali El-Remaily & Ali M. Ali. (2022) Efficient and Recoverable Bio-Organic Catalyst Cysteine for Synthesis, Docking Study, and Antifungal Activity of New Bio-Active 3,4-Dihydropyrimidin-2(1 H )-ones/thiones Under Microwave Irradiation . ACS Omega 7:26, pages 22839-22849.
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Ali Rahmatpour & Ghazaleh Donyapeyma. (2022) Poly( N ‐vinyl‐2‐pyrrolidone)‐supported ferric chloride: An effective reusable heterogeneous catalyst for one‐pot synthesis of 3,4‐dihydropyrimidin‐2( 1 H )‐ones/thiones via three‐component Biginelli reaction . Journal of Heterocyclic Chemistry 59:6, pages 997-1006.
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Tejas M. Dhameliya, Prinsa R. Nagar, Kaushikkumar A. Bhakhar, Hevankumar R. Jivani, Bhavya J. Shah, Khushi M. Patel, Vaishnavi S. Patel, Archita H. Soni, Lipi P. Joshi & Normi D. Gajjar. (2022) Recent advancements in applications of ionic liquids in synthetic construction of heterocyclic scaffolds: A spotlight. Journal of Molecular Liquids 348, pages 118329.
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M. BHASKARA RAO & B. VENKATESWARA RAO. (2022) One-Pot Synthesis and Characterization of 3,4-Dihydropyrimidin-2(1H)-one Derivatives using Sulphonated Reduced Graphene Oxide Nanoparticles via Biginelli Cyclocondensation and its Cytotoxic Studies. Asian Journal of Chemistry 34:3, pages 627-634.
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Samahe Sadjadi & Fatemeh Koohestani. (2020) Bentonite with high loading of ionic liquid: A potent non-metallic catalyst for the synthesis of dihydropyrimidinones. Journal of Molecular Liquids 319, pages 114393.
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Lakha V Chopda & Pragnesh N. Dave. (2020) Fe(III)/Bentonite as a Heterogeneous Catalyst for the Synthesis of 3,4‐dihydropyrimidin‐2‐(1H)‐ones. ChemistrySelect 5:44, pages 14161-14167.
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Mahmoud Abd El Aleem Ali Ali El‐Remaily & Omar M. Elhady. (2020) Green Bio‐organic and Recoverable Catalyst Taurine (2‐aminoethanesulfonic acid) for Synthesis of Bio‐active Compounds 3,4‐Dihydropyrimidin Derivatives in Aqueous Medium.. ChemistrySelect 5:39, pages 12098-12102.
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Shady M. El-Dafrawy, Reda S. Salama, Sohier A. El-Hakam & Salem E. Samra. (2020) Bimetal-organic frameworks (Cu -Cr –MOF) as a stable and efficient catalyst for synthesis of 3, 4-dihydropyrimidin-2-one and 14-phenyl-14H-dibenzo [a, j] xanthene. Journal of Materials Research and Technology 9:2, pages 1998-2008.
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Reyniel Ben Carvalho & Shreerang V. Joshi. (2019) Solvent and catalyst free synthesis of 3,4-dihydropyrimidin-2(1 H )-ones/thiones by twin screw extrusion . Green Chemistry 21:8, pages 1921-1924.
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Rajendra V. Patil, Jagdish U. Chavan, Dipak S. Dalal, Vaishali S. Shinde & Anil G. Beldar. (2019) Biginelli Reaction: Polymer Supported Catalytic Approaches. ACS Combinatorial Science 21:3, pages 105-148.
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Sofiane Mekki, Lahcen Krabia, Saleh Mahmoud Saleh Mohamed & Salima Saidi-Besbes. (2018) Synthesis of 3,4-Dihydropyrimidin-2(1H)-one Derivatives Using Activated Montmorillonite as Catalyst. Letters in Organic Chemistry 16:1, pages 59-65.
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M. Pasupathi, N. Santhi, M.P. Pachamuthu, G. Alamelu Mangai & C. Ragupathi. (2018) Aluminium and titanium modified mesoporous TUD-1: A bimetal acid catalyst for Biginelli reaction. Journal of Molecular Structure 1160, pages 161-166.
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Mehdi Sheykhan, Asieh Yahyazadeh & Leila Ramezani. (2017) A novel cooperative Lewis acid/Brønsted base catalyst Fe3O4@SiO2-APTMS-Fe(OH)2: An efficient catalyst for the Biginelli reaction. Molecular Catalysis 435, pages 166-173.
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Sandeep P. Bahekar, Prashant B. Sarode, Murlidhar P. Wadekar & Hemant S. Chandak. (2017) Simple and efficient synthesis of 3,4-dihydropyrimidin-2(1 H )-thiones utilizing l -proline nitrate as a proficient, recyclable and eco-friendly catalyst. Journal of Saudi Chemical Society 21:4, pages 415-419.
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Hela Slimi, Younes Moussaoui & Ridha ben Salem. (2016) Synthesis of 3,4-dihydropyrimidin-2(1H)-ones/thiones via Biginelli reaction promoted by bismuth(III)nitrate or PPh3 without solvent. Arabian Journal of Chemistry 9, pages S510-S514.
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Deepa Dumbre, Mohammad Hassan Amin, Qing Loh, Vasant R. Choudahry, P. R. Selvakannan & Suresh K. Bhargava. (2016) Nanocrystalline FeOCl x grafted MCM-41 as active mesoporous catalyst for the solvent-free multi-condensation reaction . RSC Advances 6:73, pages 69334-69342.
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Zarrin Ghasemi, Farzaneh Farshbaf Orafa, Mahtab Pirouzmand, Gholamreza Zarrini, Behnaz Nikzad Kojanag & Roya Salehi. (2015) Zn2+/MCM-41 catalyzed Biginelli reaction of heteroaryl aldehydes and evaluation of the antimicrobial activity and cytotoxicity of the pyrimidone products. Tetrahedron Letters 56:46, pages 6393-6396.
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K. Aswin, S. Sheik Mansoor, K. Logaiya & S.P.N. Sudhan. (2014) Triphenylphosphine: An efficient catalyst for the synthesis of 4,6-diphenyl-3,4-dihydropyrimidine-2(1H)-thione under thermal conditions. Journal of King Saud University - Science 26:2, pages 141-148.
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Eskandar Kolvari, Nadiya Koukabi & Ozra Armandpour. (2014) A simple and efficient synthesis of 3,4-dihydropyrimidin-2-(1H)-ones via Biginelli reaction catalyzed by nanomagnetic-supported sulfonic acid. Tetrahedron 70:6, pages 1383-1386.
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Majid M. Heravi, Shima Asadi & Boshra Malekzadeh Lashkariani. (2013) Recent progress in asymmetric Biginelli reaction. Molecular Diversity 17:2, pages 389-407.
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Eskandar Kolvari & Maryam Mirzaeeyan. (2013) Al(NO 3 ) 3  · 9H 2 O: An Efficient Catalyst for the One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1 H )-ones Both under Reflux or Solvent-Free Conditions . Journal of Chemistry 2013, pages 1-5.
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Larry Yet. 2012. 393 420 .
Eskandar Kolvari, Mohammad Ali Zolfigol & Maryam Mirzaeean. (2012) Aluminium Nitrate Nonahydrate (Al(NO 3 ) 3 ⋅9 H 2 O): An Efficient Oxidant Catalyst for the One‐Pot Synthesis of Biginelli Compounds from Benzyl Alcohols . Helvetica Chimica Acta 95:1, pages 115-119.
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Hossein A. Oskooie, Majid M. Heravi, Narges Karimi & Maryam H. Monjezy. (2011) ChemInform Abstract: FeCl 3 Immobilized in Al‐MCM 41: An Efficient Catalyst System for the Biginelli Reaction. . ChemInform 42:32.
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