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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 3, 1973 - Issue 4
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Original Articles

Reduction and Reductive Alkylation of α-tert-Butylthio Carbonyl Compounds. An Efficient Method for Stepwise α-Alkylation of Esters, Nitriles and Ketones Via the α-Tert-Butylthio Derivatives

S. Kamata Shionogi Research Laboratory, Shionogi & Co., Ltd., Fukushima-ku, Osaka, 553, Japan
,
Shoichiro Uyeo Shionogi Research Laboratory, Shionogi & Co., Ltd., Fukushima-ku, Osaka, 553, Japan
,
N. Haga Shionogi Research Laboratory, Shionogi & Co., Ltd., Fukushima-ku, Osaka, 553, Japan
&
W. Nagata Shionogi Research Laboratory, Shionogi & Co., Ltd., Fukushima-ku, Osaka, 553, Japan
Pages 265-272 | Received 06 Jun 1973, Published online: 05 Dec 2006

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Seizi Kurozumi, Takeshi Toru, Makiko Kobayashi & Sachio Ishimoto. (1977) A New Desulfurization Method: Application to the Synthesis of 11-Deoxyprostaglandin E2 . Synthetic Communications 7:7, pages 427-432.
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Miguel Yus & Francisco Foubelo. 2008. Modern Reduction Methods. Modern Reduction Methods 419 445 .
B Jolivet & D Uguen. (2002) Should anionised benzylic sulfones be considered as carbenoids?. Tetrahedron Letters 43:44, pages 7907-7911.
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Jeffrey M. Manthorpe & James L. Gleason. (2001) Stereoselective Generation of E- and Z-Disubstituted Amide Enolates. Reductive Enolate Formation from Bicyclic Thioglycolate Lactams. Journal of the American Chemical Society 123:9, pages 2091-2092.
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Jia-Liang Zhu, Kak-Shan Shia & Hsing-Jang Liu. (1999) Reductive alkylation of ?-cyano ketones induced by samarium iodide. Tetrahedron Letters 40:39, pages 7055-7058.
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Hsing-Jang Liu, Jia-Liang Zhu & Kak-Shan Shia. (1998) Lithium naphthalenide induced reductive alkylation of ?-cyano ketones. A general method for regiocontrol of ?, ?-dialkylation of ketones. Tetrahedron Letters 39:24, pages 4183-4186.
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Ana B. Bueno, M. Carmen Carre?o, Jos?L. Garc?a Ruano & Chafiq Hamdouchi. (1995) Asymmetric synthesis of cyclohex-2-enols: The examples of seudenol and analogues. Tetrahedron: Asymmetry 6:6, pages 1237-1240.
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Frank S. GuziecJr.Jr. & Lynn J. Guziec. 1995. Comprehensive Organic Functional Group Transformations. Comprehensive Organic Functional Group Transformations 381 401 .
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Stephen F. Martin. (1980) Methodology for the construction of quaternary carbon centers. Tetrahedron 36:4, pages 419-460.
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Rudolf Gompper & Hans‐Ulrich Wagner. (2003) The Concept of Allopolarization. Effects of Substituents on the Reactions of Ambifunctional Anions. Angewandte Chemie International Edition in English 15:6, pages 321-333.
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Rudolf Gompper & Hans‐Ulrich Wagner. (2006) Das Allopolarisierungs‐Prinzip. Substituenteneinflüsse auf Reaktionen ambifunktioneller Anionen. Angewandte Chemie 88:12, pages 389-401.
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Dieter Seebach & Manfred Teschner. (2006) Herstellung α‐thiolierter Carbonylverbindungen. Chemische Berichte 109:5, pages 1601-1616.
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D.W. Slocum. (1975) Lithium. Journal of Organometallic Chemistry 95, pages 1-137.
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Stephen S. Washburne. (1974) Silicon - application to organic synthesis annual survey covering the year 1973. Journal of Organometallic Chemistry 82, pages 155-211.
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Stephen S. Washburne. (1974) Silicon - application to organic synthesis. Journal of Organometallic Chemistry 83, pages 155-211.
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S. KAMATA, S. UYEO, N. HAGA & W. NAGATA. (2016) ChemInform Abstract: REDUCTION AND REDUCTIVE ALKYLATION OF ALPHA‐TERT.‐BUTYLTHIO CARBONYL COMPOUNDS, AN EFFICIENT METHOD FOR STEPWISE ALPHA‐ALKYLATION OF ESTERS, NITRILES AND KETONES VIA THE ALPHA‐TERT.‐BUTYLTHIO DERIVATIVES. Chemischer Informationsdienst 5:7.
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Robert M. Coates, H.Dale Pigott & Janet Ollinger. (1974) Alkylation and reduction-alkylation of ?-phenylthio ketones and aldehydes. Tetrahedron Letters 15:45, pages 3955-3958.
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