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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 14, 1984 - Issue 1
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Original Articles

A Preparative Gas-Solid-Phase Synthesis of Acetyl Hypofluorite

Douglas M. Jewett Cyclotron/PET Facility, Division of Nuclear Medicine University of Michigan Medical School 3480 Kresge I, Box 056 Ann Arbor, Michigan, 48109
,
Jan F. Potocki Cyclotron/PET Facility, Division of Nuclear Medicine University of Michigan Medical School 3480 Kresge I, Box 056 Ann Arbor, Michigan, 48109
&
Richard E. Ehrenkaufer Cyclotron/PET Facility, Division of Nuclear Medicine University of Michigan Medical School 3480 Kresge I, Box 056 Ann Arbor, Michigan, 48109
Pages 45-51 | Published online: 05 Dec 2006

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N. Satyamurthy, G.T. Blda, H.C. Padgett & J.R. Barrio. (1985) On the Stereoselectivity of Fluorine and Acetylhypofluorite Additions to Glycals: The Synthesis of 2-Deoxy-2-Fldorohexoses. Journal of Carbohydrate Chemistry 4:4, pages 489-512.
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Articles from other publishers (32)

Hongzhuang Zhang, Haibo Mei, Mengqing Li, Zhulan Liu, Jianlin Han & Yunfeng Cao. (2023) A review: Deoxy-fluorination of galactose – One of lignocellulosic biomass hydrolysates. Industrial Crops and Products 197, pages 116671.
Crossref
Peer Kirsch. 2013. Modern Fluoroorganic Chemistry. Modern Fluoroorganic Chemistry 299 350 .
Peer Kirsch. 2013. Modern Fluoroorganic Chemistry. Modern Fluoroorganic Chemistry 25 106 .
Zvi RappoportShlomo Rozen. 2010. Patai's Chemistry of Functional Groups. Patai's Chemistry of Functional Groups.
Izabela Fokt, Slawomir Szymanski, Stanislaw Skora, Marcin Cybulski, Timothy Madden & Waldemar Priebe. (2009) d-Glucose- and d-mannose-based antimetabolites. Part 2. Facile synthesis of 2-deoxy-2-halo-d-glucoses and -d-mannoses. Carbohydrate Research 344:12, pages 1464-1473.
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Michael J. Adam. (2002) Radiohalogenated carbohydrates for use in PET and SPECT. Journal of Labelled Compounds and Radiopharmaceuticals 45:2, pages 167-180.
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Takashi Hayashi, Brion W Murray, Ruo Wang & Chi-Huey Wong. (1997) A chemoenzymatic synthesis of UDP-(2-deoxy-2-fluoro)galactose and evaluation of its interaction with galactosyltransferase. Bioorganic & Medicinal Chemistry 5:3, pages 497-500.
Crossref
Shlomo Rozen. (1996) Selective Fluorinations by Reagents Containing the OF Group. Chemical Reviews 96:5, pages 1717-1736.
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Shlomo Rozen, Yifat Bareket & Moshe Kol. (1993) Solvent dependence of the synthesis and reactions of acetyl hypofluorite. Journal of Fluorine Chemistry 61:1-2, pages 141-146.
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Hermann Vyplel, Dieter Scholz, Hans Loibner, Michael Kern, Karl Bednarik & Hans Schaller. (1992) Synthesis of fluorinated analogues of lipid A. Tetrahedron Letters 33:10, pages 1261-1264.
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Marcel Guillaume, Andre Luxen, Bruno Nebeling, Mario Argentini, John C. Clark & Victor W. Pike. (1991) Recommendations for fluorine-18 production. International Journal of Radiation Applications and Instrumentation. Part A. Applied Radiation and Isotopes 42:8, pages 749-762.
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Richard J. Flanagan. 1991. New Trends in Radiopharmaceutical Synthesis, Quality Assurance, and Regulatory Control. New Trends in Radiopharmaceutical Synthesis, Quality Assurance, and Regulatory Control 279 288 .
Tsutomu Tsuchiya. 1990. Advances in Carbohydrate Chemistry and Biochemistry Volume 48. Advances in Carbohydrate Chemistry and Biochemistry Volume 48 91 277 .
M. Diksic, M. Trani & S. Nagahiro. (1989) Synthesis of 6-[18F]fluoropyridoxal and radioactivity distribution in rat at 60 min. International Journal of Radiation Applications and Instrumentation. Part B. Nuclear Medicine and Biology 16:4, pages 413-418.
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Georgii Georgievich Furin. 1989. New Fluorinating Agents in Organic Synthesis. New Fluorinating Agents in Organic Synthesis 35 68 .
Klaus Wienhard, Rainer Wagner & Wolf-Dieter HeissKlaus Wienhard, Rainer Wagner & Wolf-Dieter Heiss. 1989. PET. PET 86 119 .
Franz Oberdorfer, Birgitt‐C. Traving, Wolfgang Maier‐Borst & William E. Hull. (2006) Preparation and characterization of 2‐deoxy‐2‐[ 18 F] fluoro‐D‐galactose . Journal of Labelled Compounds and Radiopharmaceuticals 25:5, pages 465-481.
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A. Luxen, J.R. Barrio, N. Satyamurthy, G.T. Bida & M.E. Phelps. (1987) Electrophilic and nucleophilic approaches to the synthesis of 3-fluorodiazepam. Journal of Fluorine Chemistry 36:1, pages 83-92.
Crossref
. (2016) Conclusion. Journal of Cerebral Blood Flow & Metabolism 7:1_suppl, pages S28-S31.
Crossref
Karl Dax, Brigitte I. Glänzer, Gerhard Schulz & Hermann Vyplel. (1987) Reaction of acetyl hypofluorite with pyranoid and furanoid glycals. Carbohydrate Research 162:1, pages 13-22.
Crossref
H Nakai, H Matsuda, E Takara, M Diksic, E Meyer & Y L Yamamoto. (1987) Simultaneous in vivo measurement of lumped constant and rate constants in experimental cerebral ischemia using F-18 FDG.. Stroke 18:1, pages 158-167.
Crossref
H.H. Coenen, V.W. Pike, G. Stöcklin & R. Wagner. (1987) Recommendation for a practical production of [2-18F]fluoro-2-deoxy-D-glucose. International Journal of Radiation Applications and Instrumentation. Part A. Applied Radiation and Isotopes 38:8, pages 605-610.
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Kiichi Ishiwata, Tatsuo Ido, Hiroaki Nakanishi & Ren Iwata. (1987) Contamination of 2-deoxy-2-[18F]fluoro-d-mannose in the 2-deoxy-2-[18F]fluoro-d-glucose preparations synthesized from [18F]acetyl hypofluorite and [18F]F2. International Journal of Radiation Applications and Instrumentation. Part A. Applied Radiation and Isotopes 38:6, pages 463-466.
Crossref
Mirko Diksic & Dean Jolly. (1986) Synthesis of 2-deoxy-2-fluorohexoses by fluorination of glycals in aqueous media. Carbohydrate Research 153:1, pages 17-24.
Crossref
Chyng-Yann Shiue & A.P. Wolf. (1986) Factors affecting the purity of 2-deoxy-2-fluoro-D-glucose synthesized from the reactions of glycals with acetyl hypofluorite. Journal of Fluorine Chemistry 31:3, pages 255-263.
Crossref
Franz Oberdorfer, William E. Hull, Birgitt C. Traving & Wolfgang Maier-Borst. (1986) Synthesis and purification of 2-deoxy-2-[18F]fluoro-d-glucose and 2-deoxy-2-[18F]fluoro-d-mannose: characterization of products by 1H- and 19F-NMR spectroscopy. International Journal of Radiation Applications and Instrumentation. Part A. Applied Radiation and Isotopes 37:8, pages 695-701.
Crossref
Mirko Diksic, Dean Jolly & Dean Jolly. (1986) Remote operated synthesis of 2-deoxy-2-[18F]Fluoro-d-glucose. International Journal of Radiation Applications and Instrumentation. Part A. Applied Radiation and Isotopes 37:11, pages 1159-1161.
Crossref
Jorge R. Barrio, Randy E. Keen, Diane C. Chugani, Gerald Bida, Nagichettiar Satyamurthy & Michael E. Phelps. 1986. Analytical and Chromatographic Techniques in Radiopharmaceutical Chemistry. Analytical and Chromatographic Techniques in Radiopharmaceutical Chemistry 213 231 .
M. M. Vora, T. E. Boothe, R. D. Finn, P. J. Kothari, A. M. Emran, S. T. Carroll & A. J. Gilson. (2006) Multimillicurie preparation of 2‐[ 18 F]‐fluoro‐2‐deoxy‐D‐glucose via nucleophilic displacement with fluorine‐18 labelled fluoride. 1. Purification and quality control procedures . Journal of Labelled Compounds and Radiopharmaceuticals 22:9, pages 953-960.
Crossref
M. Reivich, A. Alavi, A. Wolf, J. Fowler, J. Russell, C. Arnett, R. R. MacGregor, C. Y. Shiue, H. Atkins, A. Anand, R. Dann & J. H. Greenberg. (2016) Glucose Metabolic Rate Kinetic Model Parameter Determination in Humans: The Lumped Constants and Rate Constants for [ 18 F]Fluorodeoxyglucose and [ 11 C]Deoxyglucose . Journal of Cerebral Blood Flow & Metabolism 5:2, pages 179-192.
Crossref
Chyng‐Yann Shiue, Joanna S. Fowler, Alfred P. Wolf, David Alexoff & Robert R. Macgregor. (2006) Gas‐liquid chromatographic determination of relative amounts of 2‐deoxy‐2‐flouro‐D‐glucose and 2‐deoxy‐2‐fluoro‐D‐mannose synthesized from various methods. Journal of Labelled Compounds and Radiopharmaceuticals 22:5, pages 503-508.
Crossref
D. M. JEWETT, J. F. POTOCKI & R. E. EHRENKAUFER. (2016) ChemInform Abstract: A PREPARATIVE GAS‐SOLID‐PHASE SYNTHESIS OF ACETYL HYPOFLUORITE. Chemischer Informationsdienst 15:45.
Crossref

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