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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 20
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Original Articles

Rapid, Low-Temperature Amidation of Ethyl Cyano-Acetate with Lithium Amides Derived from primary and Secondary Amines

Baburao M. Bhawal Department of Chemistry, Southern Methodist University, Dallas, TX, 75275
,
Subhash P. Khanapure Department of Chemistry, Southern Methodist University, Dallas, TX, 75275
&
Edward R. Biehl Department of Chemistry, Southern Methodist University, Dallas, TX, 75275
Pages 3235-3243 | Received 10 Sep 1990, Published online: 24 Oct 2006

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Nesma M. Bayoumy, Ahmed Fekri, Eman H. Tawfik & Ahmed A. Fadda. (2021) Synthesis, Characterization and Antimicrobial Evaluation of Some New Heterocycles Incorporating Phenothiazine Moiety. Polycyclic Aromatic Compounds 41:5, pages 982-991.
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Andrzej Manikowski & Zofia Kolarska. (2009) Facile and Versatile Room-Temperature Synthesis of N,N-Disubstituted Cyanoacetamides from Malonic Ester Chloride. Synthetic Communications 39:20, pages 3621-3638.
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Articles from other publishers (12)

Mohamed R. Elmorsy, Ehab Abdel-Latif, Safa A. Badawy & Ahmed A. Fadda. (2020) Molecular geometry, synthesis and photovoltaic performance studies over 2-cyanoacetanilides as sensitizers and effective co-sensitizers for DSSCs loaded with HD-2. Journal of Photochemistry and Photobiology A: Chemistry 389, pages 112239.
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Ahmed A. Fadda & Ramy Rabie. (2015) Cyanoacetylation of amines: recent advances in preparation methods and their synthetic uses in the formation of biologically active compounds. Research on Chemical Intermediates 42:2, pages 771-811.
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Pál Csuka, Zoltán Boros, László Őrfi, Judit Dobos, László Poppe & Gábor Hornyánszky. (2015) Chemoenzymatic route to Tyrphostins involving lipase-catalyzed kinetic resolution of 1-phenylethanamine with alkyl cyanoacetates as novel acylating agents. Tetrahedron: Asymmetry 26:12-13, pages 644-649.
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Felix Wilde, Edgar Specker, Martin Neuenschwander, Marc Nazaré, Anja Bodtke & Andreas Link. (2014) Tractable synthesis of multipurpose screening compounds with under-represented molecular features for an open access screening platform. Molecular Diversity 18:3, pages 483-495.
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Mark J Robertson, Fiona M Deane, Phillip J Robinson & Adam McCluskey. (2014) Synthesis of Dynole 34-2, Dynole 2-24 and Dyngo 4a for investigating dynamin GTPase. Nature Protocols 9:4, pages 851-870.
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Johannes L. Vrijdag, Francisca Delgado, Nerea Alonso, Wim M. De Borggraeve, Natalia Pérez-Macias & Jesus Alcázar. (2014) Practical preparation of challenging amides from non-nucleophilic amines and esters under flow conditions. Chem. Commun. 50:95, pages 15094-15097.
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Krishna Chaitanya Nadimpally, Kishore Thalluri, Nani Babu Palakurthy, Abhijit Saha & Bhubaneswar Mandal. (2011) Catalyst and solvent-free amidation of inactive esters of N-protected amino acids. Tetrahedron Letters 52:20, pages 2579-2582.
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Kristin E. Price, Claude Larrivée-Aboussafy, Brett M. Lillie, Robert W. McLaughlin, Jason Mustakis, Kevin W. Hettenbach, Joel M. Hawkins & Rajappa Vaidyanathan. (2009) Mild and Efficient DBU-Catalyzed Amidation of Cyanoacetates. Organic Letters 11:9, pages 2003-2006.
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Wei Zhou, Hai-bo Li, Chun-nian Xia, Xian-ming Zheng & Wei-xiao Hu. (2009) The synthesis and biological evaluation of some caffeic acid amide derivatives: E-2-Cyano-(3-substituted phenyl)acrylamides. Bioorganic & Medicinal Chemistry Letters 19:7, pages 1861-1865.
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Daniel L. Comins & Sajan P. Joseph. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
Lee H. Latimer. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
B. M. BHAWAL, S. P. KHANAPURE & E. R. BIEHL. (2010) ChemInform Abstract: Rapid, Low-Temperature Amidation of Ethyl Cyanoacetate (II) with Lithium Amides Derived from Primary and Secondary Amines (I).. ChemInform 22:15, pages no-no.
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