Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 1
60
Views
66
CrossRef citations to date
0
Altmetric
Original Articles

Dry Reaction Under Microwave: Condensation of Sulfones with Aldehydes on KF-Alumina

&
Pages 63-68 | Received 02 Nov 1990, Published online: 24 Sep 2006

Keep up to date with the latest research on this topic with citation updates for this article.

Read on this site (15)

Yuriy M. Markitanov, Vadim M. Timoshenko & Yuriy G. Shermolovich. (2014) β-Keto sulfones: preparation and application in organic synthesis. Journal of Sulfur Chemistry 35:2, pages 188-236.
Read now
M. Raghavendra, HalehattyS. Bhojya Naik, TangaliR. R Ravikumar Naik & BailureS. Sherigara. (2007) p-TsOH Catalysed a Facile One-Pot Synthesis of Some New Substituted [1,2,4]Triazolo[3,4-b][1,3,4] thiadiazepines under Microwave Irradiation in Solvent-Free Conditions. Phosphorus, Sulfur, and Silicon and the Related Elements 182:8, pages 1823-1831.
Read now
Shen-Yi Yu & Ya-Xian Cai. (2003) Synthesis of Polysubstituted Pyrimidines from Ketene Dithioacetals Using KF/Al2O3 Catalyst. Synthetic Communications 33:22, pages 3989-3995.
Read now
Jin-Xian Wang, Liqin Kang, Yulai Hu & Bangguo guo Wei. (2002) SYNTHESIS OF BIS(SUBSTITUTED BENZYLIDENE)CYCLOALKANONE USING SUPPORTED REAGENTS AND MICROWAVE IRRADIATION. Synthetic Communications 32:11, pages 1691-1696.
Read now
Anil S. Gajare, Dhananjay P. Sabde, Murlidhar S. Shingare & Radhika D. Wakharkar. (2002) MICROWAVE ACCELERATED TETRAHYDROPYRANYLATION AND DETETRAHYDROPYRANYLATION OF ALCOHOLS, PHENOLS, AND THIOLS CATALYZED BY HYDRATED ZIRCONIA. Synthetic Communications 32:10, pages 1549-1555.
Read now
Marimuthu Anniyappan, D. Muralidharan & Paramasivan T. Perumal. (2002) SYNTHESIS OF HANTZSCH 1,4-DIHYDROPYRIDINES UNDER MICROWAVE IRRADIATION. Synthetic Communications 32:4, pages 659-663.
Read now
Mazaahir Kidwai, Pooja Sapra, Kumar Ranjan Bhushan & Preeti Misra. (2001) MICROWAVE ASSISTED SYNTHESIS OF NOVEL 1,2,4-TRIAZINES IN “DRY MEDIA”. Synthetic Communications 31:11, pages 1639-1645.
Read now
M. Kidwai, P. Misra & K. R. Bhushan. (2001) ALUMINA-SUPPORTED SYNTHESIS OF THIADIAZOLYL THIAZOLOTHIONES. Synthetic Communications 31:6, pages 817-822.
Read now
RajenderS. Varma & Dalip Kumar. (1999) Solventless Regeneration of Ketones from Thioketones using Clay Supported Nitrate Salts and Microwave Irradiation. Synthetic Communications 29:8, pages 1333-1340.
Read now
Maryam Mirza-aghayan & MajidM. Heravi. (1999) Chromium Trioxide on H-Y Zeolite: Rapid Oxidation of Alcohols to Carbonyl Compounds in Solventless System Using Microwaves. Synthetic Communications 29:5, pages 785-789.
Read now
RajenderS. Varma & Rajender Dahiya. (1998) Microwave Thermolysis with Clayfen: Solvent-Free Oxidation of Sulfides to Sulfoxides. Synthetic Communications 28:21, pages 4087-4095.
Read now
H.M.Sampath Kumar, PradyumnaK. Mohanty, M. Suresh Kumar & J.S. Yadav. (1997) Microwave Promoted Rapid Dehydration of Aldoximes to Nitriles on a Solid Support . Synthetic Communications 27:8, pages 1327-1333.
Read now
RudolphA. Abramovitch, Quing Shi & Dariusz Bogdal. (1995) Microwave-Assisted Alkylations of Activated Methylene Groups. Synthetic Communications 25:1, pages 1-8.
Read now
Jinchang Ding, Hengjie Gu, Jinzhu Wen & Caizhen Lin. (1994) Dry Reaction Under Microwave: N—Alkylation of Saccharin on Silicagel. Synthetic Communications 24:3, pages 301-303.
Read now
RudolphA. Abramovitch. (1991) APPLICATIONS OF MICROWAVE ENERGY IN ORGANIC CHEMISTRY. A REVIEW. Organic Preparations and Procedures International 23:6, pages 683-711.
Read now

Articles from other publishers (51)

Yijiao Feng, Jing He, Yueting Wei, Ting Tang, Chuntian Li & Ping Liu. (2022) One-Pot Two-Step Strategy for Efficient Synthesis of 3-Aryl-4-(arylthio)-1 H -pyrazol-5-amines Derivatives . Chinese Journal of Organic Chemistry 42:1, pages 226.
Crossref
Yueting Wei, Ping Liu, Yali Liu, Jing He, Xuezhen Li, Shiwu Li & Jixing Zhao. (2021) NIS-promoted three-component reaction of 3-oxo-3-arylpropanenitriles with arylsulfonyl hydrazides. Organic & Biomolecular Chemistry 19:17, pages 3932-3939.
Crossref
Yaohong Zhang, Mengqiang Luo, Yan Li, Runfu Shen, Chenze Qi, Hai Wang & Kai Cheng. (2020) One-pot synthesis of β-ketosulfones from sulfonyl chloride, hydrazine hydrate and vinyl azide in water. Tetrahedron 76:48, pages 131635.
Crossref
Khaled M. Elattar, Ahmed Fekri, Nesma M. Bayoumy & Ahmed A. Fadda. (2017) Sulfones in heterocyclic synthesis: advances in the chemistry of phenyl sulfonylacetophenone. Research on Chemical Intermediates 43:7, pages 4227-4264.
Crossref
Rania S. Ali, R. R. Al Harthi, H. A. Saad & M. A. Amin. (2017) Synthesis of some new fused 1,2,4-triazines and their antimicrobial activity. Russian Journal of General Chemistry 86:12, pages 2906-2913.
Crossref
Kapil S. Pandit, Ravindra V. Kupwade, Pramod V. Chavan, Uday V. Desai, Prakash P. Wadgaonkar & Kisan M. Kodam. (2016) Problem Solving and Environmentally Benign Approach toward Diversity Oriented Synthesis of Novel 2-Amino-3-phenyl (or Alkyl) Sulfonyl-4 H -chromenes at Ambient Temperature . ACS Sustainable Chemistry & Engineering 4:6, pages 3450-3464.
Crossref
Ali Gharib. 2014. Green Chemistry: Synthesis of Bioactive Heterocycles. Green Chemistry: Synthesis of Bioactive Heterocycles 69 104 .
Qing Chao Jia, Yan Jun Chen & Hong Min Hou. (2012) Microwave-Assisted Synthesis of Azo Aromatic Diacyl Chlorides. Advanced Materials Research 524-527, pages 1702-1705.
Crossref
David I. MageeSame RatshonkaJessica McConaghyMaggie Hood. (2012) Synthesis of β- and β,β-substituted Morita–Baylis–Hillman adducts using a two-step protocol. Canadian Journal of Chemistry 90:5, pages 450-463.
Crossref
Qi Han, Hui-Yin Li, Yossi Zafrani, Eytan Gershonov & Ishay Columbus. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
Hosam A. Saad, Mohamed M. Youssef & Mosselhi A. Mosselhi. (2011) Microwave Assisted Synthesis of Some New Fused 1,2,4-Triazines Bearing Thiophene Moieties With Expected Pharmacological Activity. Molecules 16:6, pages 4937-4957.
Crossref
Anshu Dandia, Kapil Arya, Sarita Khaturia & Anuj Kumar Jain. (2010) Microwave-induced preparation of biologically important benzothiazolo[2,3-b]quinazolines, and comparison with ultrasonic and classical heating. Monatshefte für Chemie - Chemical Monthly 141:9, pages 979-985.
Crossref
Shengyong You, Jianying Li & Mingzhong Cai. (2009) A facile stereoselective synthesis of (Z)-α-arylsulfonyl-α,β-unsaturated ketones. Tetrahedron 65:34, pages 6863-6867.
Crossref
M Raghavendra, Halehatty S. Bhojya Naik & Bailure S Sherigara. (2007) Microwave-assisted one-pot synthesis of some new furo[2,3- b ]quinolines using potassium carbonate under solvent-free conditions . Canadian Journal of Chemistry 85:12, pages 1041-1044.
Crossref
N. Suryakiran, T. Srikanth Reddy, K. Asha Latha, P. Prabhakar, K. Yadagiri & Y. Venkateswarlu. (2006) An expeditious synthesis of 3-amino 2H-pyrazoles promoted by methanesulphonic acid under solvent and solvent free conditions. Journal of Molecular Catalysis A: Chemical 258:1-2, pages 371-375.
Crossref
Anshu Dandia, Ruby Singh & Sarita Khaturia. (2006) Microwave enhanced solid support synthesis of fluorine containing benzopyrano-triazolo-thiadiazepines as potent anti-fungal agents. Bioorganic & Medicinal Chemistry 14:5, pages 1303-1308.
Crossref
Mohamed Zahouily, Mohamed Salah, Bouchaib Bahlaouane, Ahmed Rayadh, Abdelaziz Houmam, Emad A Hamed & Saı̈d Sebti. (2004) Solid catalysts for the production of fine chemicals: the use of natural phosphate alone and doped base catalysts for the synthesis of unsaturated arylsulfones. Tetrahedron 60:7, pages 1631-1635.
Crossref
V. K. Ahluwalia & M. KidwaiV. K. Ahluwalia & M. Kidwai. 2004. New Trends in Green Chemistry. New Trends in Green Chemistry 59 72 .
Mohamed Zahouily, Mohamed Salah, Jamal Bennazha, Ahmed Rayadh & Saı̈d Sebti. (2003) Na2CaP2O7, a new catalyst for the synthesis of unsaturated arylsulfones. Tetrahedron Letters 44:16, pages 3255-3257.
Crossref
Jian-Ping Li, Ping Liu, Yu-Lu Wang & Qian-Fu Luo. (2019) Rapid Synthesis of 1,4-Diaryl Thiosemicarbazides using Microwave Technology. Journal of Chemical Research 2001:11, pages 488-489.
Crossref
Qi Han & Hui-Yin Li. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
M Kidwai, P Sapra, P Misra, R.K Saxena & M Singh. (2001) Microwave assisted solid support synthesis of novel 1,2,4-triazolo[3,4-b]-1,3,4-thiadiazepines as potent antimicrobial agents. Bioorganic & Medicinal Chemistry 9:2, pages 217-220.
Crossref
Kathrin-Maria Roy. 2000. Ullmann's Encyclopedia of Industrial Chemistry. Ullmann's Encyclopedia of Industrial Chemistry.
Mark Woods, Nuno Monteiro & Geneviève Balme. (2000) The Effect of the Carbon Ligand on the Reaction of Organozinc Reagents in the Synthesis of Substituted 2,5-Dihydrofurans: A Rare Example of An Uncatalysed Allylic-Substitution Reaction Involving Alkyl Zinc Halides. European Journal of Organic Chemistry 2000:9, pages 1711-1718.
Crossref
Rajender S. Varma. (2009) Solvent‐free synthesis of heterocyclic compounds using microwaves. Journal of Heterocyclic Chemistry 36:6, pages 1565-1571.
Crossref
András Vass, József Dudás & Rajender S. Varma. (1999) Solvent-free synthesis of N-sulfonylimines using microwave irradiation. Tetrahedron Letters 40:27, pages 4951-4954.
Crossref
Rajender S. Varma & Rajender Dahiya. (1998) An Expeditious and Solvent-Free Synthesis of 2-Amino-Substituted Isoflav-3-enes Using Microwave Irradiation. The Journal of Organic Chemistry 63:22, pages 8038-8041.
Crossref
Rajender S. Varma & Rajender Dahiya. (1998) Sodium borohydride on wet clay: Solvent-free reductive amination of carbonyl compounds using microwaves. Tetrahedron 54:23, pages 6293-6298.
Crossref
Rajender S. Varma & Rajender Dahiya. (1998) Copper(II) nitrate on clay (claycop)-hydrogen peroxide: Selective and solvent-free oxidations using microwaves. Tetrahedron Letters 39:11, pages 1307-1308.
Crossref
Rajender S. Varma & Kannan P. Naicker. (1998) Hydroxylamine on Clay: a Direct Synthesis of Nitriles from Aromatic Aldehydes Using Microwaves Under Solvent-Free Conditions. Molecules Online 2:3, pages 94-96.
Crossref
Rajender S. Varma, Rajender Dahiya & Rajesh K. Saini. (1997) Solid state regeneration of ketones from oximes on wet silica supported sodium periodate using microwaves. Tetrahedron Letters 38:51, pages 8819-8820.
Crossref
Rajender S. Varma, Rajender Dahiya & Rajesh K. Saini. (1997) Iodobenzene diacetate on alumina: Rapid oxidation of alcohols to carbonyl compounds in solventless system using microwaves. Tetrahedron Letters 38:40, pages 7029-7032.
Crossref
Rajender S. Varma, Rajesh K. Saini & Harshadas M. Meshram. (1997) Selective oxidation of sulfides to sulfoxides and sulfones by microwave thermolysis on wet silica-supported sodium periodate. Tetrahedron Letters 38:37, pages 6525-6528.
Crossref
Rajender S. Varma & Harshadas M. Meshram. (1997) Solid state deoximation with ammonium persulfate-silica gel: Regeneration of carbonyl compounds using microwaves. Tetrahedron Letters 38:31, pages 5427-5428.
Crossref
Rajender S. Varma, Rajender Dahiya & Sudhir Kumar. (1997) Microwave-assisted Henry reaction: Solventless synthesis of conjugated nitroalkenes. Tetrahedron Letters 38:29, pages 5131-5134.
Crossref
George W. Kabalka & Richard M. Pagni. (1997) Organic reactions on alumina. Tetrahedron 53:24, pages 7999-8065.
Crossref
Rajender S. Varma, Rajender Dahiya & Sudhir Kumar. (1997) Clay catalyzed synthesis of imines and enamines under solvent-free conditions using microwave irradiation. Tetrahedron Letters 38:12, pages 2039-2042.
Crossref
P Kumar & K C Gupta. (1996) Microwave Assisted Synthesis of S -Trityl and S -Acylmercaptoalkanols, Nucleosides and Their Deprotection . Chemistry Letters 25:8, pages 635-636.
Crossref
Hubert Maehr & Roxana Yang. (1996) A convergent synthesis of Ro24-5913, a novel leukotriene D4 antagonist. Tetrahedron Letters 37:31, pages 5445-5448.
Crossref
S. Caddick. (1995) Microwave assisted organic reactions. Tetrahedron 51:38, pages 10403-10432.
Crossref
. 1995. Compendium of Organic Synthetic Methods. Compendium of Organic Synthetic Methods 276 559 .
Diego A. Torres & John P. Ferraris. (1994) Knoevenagel-like condensations with highly stabilized active methylene compounds. Tetrahedron Letters 35:41, pages 7589-7592.
Crossref
Rudolph A. Abramovitch & Kaliappan Iyanar. (1994) Organosolv Pulping Using a Microwave Oven. hfsg 48:4, pages 349-354.
Crossref
Francesco Fringuelli, Giosanna Pani, Oriana Piermatti & Ferdinando Pizzo. (1994) Condensation reactions in water of active methylene compounds with arylaldehydes. One-pot synthesis of flavonols.. Tetrahedron 50:39, pages 11499-11508.
Crossref
Rajender S. Varma, Arnab K. Chatterjee & Manju Varma. (1993) Alumina-mediated microwave thermolysis: A new approach to deprotection of benzyl esters. Tetrahedron Letters 34:29, pages 4603-4606.
Crossref
Rajender S. Varma, Jagannath B. Lamture & Manju Varma. (1993) Alumina-mediated cleavage of -butyldimethylsilyl ethers. Tetrahedron Letters 34:19, pages 3029-3032.
Crossref
Rajender S. Varma, Arnab K. Chatterjee & Manju Varma. (1993) Alumina-mediated deacetylation of benzaldehyde diacetates. A simple deprotection method. Tetrahedron Letters 34:20, pages 3207-3210.
Crossref
Andrés Molina, Juan J. Vaquero, José L. García-Navio & Julio Alvarez-Builla. (1993) One-pot Graebe-Ullmann synthesis of γ-carbolines under microwave irradiation. Tetrahedron Letters 34:16, pages 2673-2676.
Crossref
Raymond J. Giguere. (2011) Microwave-Assisted Organic Synthesis. MRS Proceedings 269.
Crossref
Elisabeth A. Schmittling & J.Scott Sawyer. (1991) Selective desilylation of -butyldimethylsilyl ethers of phenols using potassium fluoride-alumina and ultrasound. Tetrahedron Letters 32:49, pages 7207-7210.
Crossref
D. VILLEMIN & A. B. ALLOUM. (2010) ChemInform Abstract: Dry Reaction Under Microwave: Condensation of Sulfones (I) with Aldehydes (II) on KF‐Alumina.. ChemInform 22:42.
Crossref

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.