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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 1
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Original Articles

Sulfuric Acid Adsorbed on Silica Gel. An Efficient Catalyst for the Tetrahydropyranylation of Alcohols

Flavio Chávez Syntex S.A. de C.V. Chemical Division Technical Services Department, Apartado Postal 517, Cuernavaca, Mor., 62000, México
&
Raul Godinez Syntex S.A. de C.V. Chemical Division Technical Services Department, Apartado Postal 517, Cuernavaca, Mor., 62000, México
Pages 159-164 | Received 15 Jul 1991, Published online: 23 Sep 2006

Citations (33)

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Nasser Montazeri & Kurosh Rad-Moghadam. (2004) A CONVENIENT SYNTHESIS OF SUBSTITUTED QUINAZOLIN-4(3H)-ONES UNDER MICROWAVE AND SOLVENT-FREE CONDITIONS. Phosphorus, Sulfur, and Silicon and the Related Elements 179:12, pages 2533-2536.
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MajidM. Heravi, Navid Ramezanian, MajidM. Sadeghi & Mitra Ghassemzadeh. (2004) SYNTHESIS OF [1,3,4]THIADIAZOLO[2,3-C][1,2,4]TRIAZIN-4-ONES USING SULFURIC ACID SUPPORTED ONTO SILICA GEL IN SOLVENTLESS SYSTEM. Phosphorus, Sulfur, and Silicon and the Related Elements 179:8, pages 1469-1472.
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Ajoy K. Banerjee, Po S. Poon & Manuel S. Laya. (2003) A New Synthesis of 4-Methylene-10-methyl-Δ8,9-carbomethoxy-trans-decalin. Synthetic Communications 33:11, pages 1929-1936.
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M. M. Heravi, M. Bakherad, M. Rahimzadeh & M. Bakavoli. (2002) Solid Acid Induced Cyclocondensation: A Facile, One-Pot Synthesis of 7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazines. Phosphorus, Sulfur, and Silicon and the Related Elements 177:10, pages 2403-2407.
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MajidM. Heravi, Dariush Ajami And & Mitra Ghassemzadeh. (1999) Solvent free Tetrahydropyranylation of Alcohols and Phenols over Sulfuric Acid Adsorbed on Silica Gel. Synthetic Communications 29:6, pages 1013-1016.
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Zhengong Li & A. Ganesan. (1998) Poly(4-Vinylpyridinium P-Toluenesulfonate) as a Polymer-Supported Catalyst for Hydrolysis of Tetrahydropyranyl Ethers. Synthetic Communications 28:17, pages 3209-3212.
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Anjana Sarkart, OmprakashS. Yemult, B.P. Bandgar, N.B. Gaikwad & PrakashP. Wadgaonkar. (1996) SULFATED ZIRCONIA AS AN EFFICIENT CATALYST FOR TETRAHYDRO PYRANYLATION AND ACETALIZATION. Organic Preparations and Procedures International 28:5, pages 613-617.
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M. Ghiaci & Y. Bayat. (1996) SYNTHESIS AND CONFORMATIONAL PROPERTIES OF 2,2′-DIHYDROXY-9,9′-BIANTHRYL. Organic Preparations and Procedures International 28:5, pages 609-612.
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B.P. Bandgar, S.R. Jagtap, B.B. Aghade & P.P. Wadgaonkar. (1995) Envirocat EPZG® as a New Heterogenous Catalyst for the Solvent-Free Tetrahydropyranylation of Alcohols and Phenols. Synthetic Communications 25:15, pages 2211-2215.
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Flavio Chávez, Silvia Suárez & MiguelA. Díaz. (1994) Sulfuric Acid Adsorbed on Silica Gel. A Multipurpose Acid Catalyst. Synthetic Communications 24:16, pages 2325-2339.
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Articles from other publishers (23)

Rama Moorthy Appa, Jangam Lakshmidevi, S. Siva Prasad, Bandameeda Ramesh Naidu, Manchala Narasimhulu & Katta Venkateswarlu. (2018) HClO 4 ⋅SiO 2 -Catalyzed Mechanochemical Protocol: An Effective, Economical and Eco-friendly Preparation of N -( tert -butylsulfinyl)imines . ChemistrySelect 3:40, pages 11236-11240.
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Brijesh Kumar, Mushtaq A. Aga, Abdul Rouf, Bhahwal A. Shah & Subhash C. Taneja. (2014) Tetrahydropyranyl ether (THPE) formation in hydroxyl group protection and conversion to other useful functionalities. RSC Adv. 4:40, pages 21121-21130.
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Hooshang Vahedi, Ghadir Rajabzadeh & Fahimeh Farvandi. (2010) Facile synthesis of [1,2,4]triazino[4,3-b][1,2,4,5]tetrazepin derivatives by a one-pot reactions using 4-amino-3-hydrazinyl-6-methyl-1,2,4-triazin-5(4H)-one. Chinese Chemical Letters 21:12, pages 1419-1422.
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Giovanni Sartori & Raimondo Maggi. (2010) Update 1 of: Protection (and Deprotection) of Functional Groups in Organic Synthesis by Heterogeneous Catalysis. Chemical Reviews 110:3.
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Ahmed Kamal, M Naseer A Khan, Y VV Srikanth & K Srinivasa Reddy. (2008) Al(OTf) 3 — A highly efficient catalyst for the tetrahydropyranylation of alcohols under solvent-free conditions . Canadian Journal of Chemistry 86:12, pages 1099-1104.
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Farhad Shirini, Mohammad Ali Zolfigol & Abdol-Reza Abri. (2007) Regioselective tetrahydropyranylation of alcohols catalyzed by Fe(HSO4)3. Chinese Chemical Letters 18:7, pages 803-806.
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Farhad Shirini, Mohammad Ali Zolfigol & Masoumeh Abedini. (2005) Silylation and Tetrahydropyranylation of Alcohols Catalyzed by Al(HSO 4 ) 3 . Bulletin of the Chemical Society of Japan 78:11, pages 1982-1985.
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Yan-Guang Wang, Xiao-Xing Wu & Zhi-Yong Jiang. (2004) A mild and efficient selective tetrahydropyranylation of primary alcohols and deprotection of THP ethers of phenols and alcohols using PdCl2(CH3CN)2 as catalyst. Tetrahedron Letters 45:14, pages 2973-2976.
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Giovanni Sartori, Roberto Ballini, Franca Bigi, Giovanna Bosica, Raimondo Maggi & Paolo Righi. (2003) Protection (and Deprotection) of Functional Groups in Organic Synthesis by Heterogeneous Catalysis. Chemical Reviews 104:1, pages 199-250.
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Bahman Tamami & Kaveh Parvanak Borujeny. (2004) Chemoselective tetrahydropyranylation of alcohols and phenols using polystyrene supported aluminium chloride as a catalyst. Tetrahedron Letters 45:4, pages 715-718.
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Ajoy K Banerjee, M S Laya & W J Vera. (2001) Silica gel in organic synthesis. Russian Chemical Reviews 70:11, pages 971-990.
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Quan Zhuang & Jack M Miller. (2001) One-pot sol-gel synthesis of sulfated ZrO 2 -SiO 2 catalysts for alcohol dehydration . Canadian Journal of Chemistry 79:8, pages 1220-1223.
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Brad R Henke, David H Drewry, Stacey A Jones, Eugene L Stewart, Susan L Weaver & Robert W Wiethe. (2001) 2-Amino-4,6-diarylpyridines as novel ligands for the estrogen receptor. Bioorganic & Medicinal Chemistry Letters 11:14, pages 1939-1942.
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Yung-Son Hon, Chia-Fu Lee, Rong-Jiunn Chen & Ping-Hui Szu. (2001) Acetonyltriphenylphosphonium bromide and its polymer-supported analogues as catalysts in protection and deprotection of alcohols as alkyl vinyl ethers. Tetrahedron 57:28, pages 5991-6001.
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Xiao-jun Wang, Jonathan Tan & Li Zhang. (2000) Regioselective Synthesis of Unsymmetrical 3,5-Dialkyl-1-arylpyrazoles. Organic Letters 2:20, pages 3107-3109.
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A.K. Banerjee & M. Laya-Mimo. 2000. Bioactive Natural Products (Part E). Bioactive Natural Products (Part E) 175 213 .
Yung-Son Hon & Chia-Fu Lee. (1999) Acetonyltriphenylphosphonium bromide in organic synthesis: An extremely efficient catalyst for the protection and deprotection of alcohols as alkyl vinyl ethers. Tetrahedron Letters 40:12, pages 2389-2392.
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David H. Drewry, Diane M. Coe & Steve Poon. (1999) Solid-supported reagents in organic synthesis. Medicinal Research Reviews 19:2, pages 97-148.
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Marcel Temciuc, Anna-Britta Hörnfeldt & Salo Gronowitz. (1996) ON THE SYNTHESES OF SOME TRITHIENYL METHANES AND TRITHIENYLMETHYL CARBENIUM IONS. Heterocyclic Communications 2:2.
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Vladimir A Basiuk. (1995) Organic reactions on the surface of silicon dioxide: synthetic applications. Russian Chemical Reviews 64:11, pages 1003-1019.
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Marcel Temciuc, Anna-Britta Hörnfeldt & Salo Gronowitz. (1995) ON THE SYNTHESES OF SOME TRITHIENYL METHANES AND TRITHIENYLMETHYL CARBENIUM IONS. Heterocyclic Communications 1:5-6.
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. 1995. Compendium of Organic Synthetic Methods. Compendium of Organic Synthetic Methods 16 53 .
F. CHAVEZ & R. GODINEZ. (2010) ChemInform Abstract: Sulfuric Acid Adsorbed on Silica Gel. An Efficient Catalyst for the Tetrahydropyranylation of Alcohols.. ChemInform 23:23.
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