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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 8
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Original Articles

Cleavage or Acetyl-de-alkylation of 4-Methoxybenzyl (MPM) Ethers Using Acetic Acid

Kevin J. Hodgetts Department of Chemistry and Applied Chemistry, University of Salford, Salford, M5 4WT, U.K.
&
Timothy W. Wallace Department of Chemistry and Applied Chemistry, University of Salford, Salford, M5 4WT, U.K.
Pages 1151-1155 | Received 31 Aug 1993, Published online: 23 Sep 2006

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Anusuya Choudhury, Michael E. Pierce & Pat N. Confalone. (2001) OXIDATIVE REMOVAL OF p-METH-OXYBENZYL-AMINO PROTECTING GROUP IN THE PRESENCE OF A PROXIMAL HYDROXY FUNCTION: A SOLUTION TO A PROCESS PROBLEM IN SUSTIVA® (EFAVIRENZ) SYNTHESIS. Synthetic Communications 31:23, pages 3707-3714.
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Articles from other publishers (20)

Laura Stief & Andreas Speicher. (2021) Setup of 4‐Prenylated Quinolines through Suzuki‐Miyaura Coupling for the Synthesis of Aurachins A and B. Advanced Synthesis & Catalysis 364:1, pages 158-164.
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Yingjie Wang & Biao Yu. (2021) Total Syntheses of Aturanosides A and B. Organic Letters 23:17, pages 6680-6684.
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Huidan Huang, Jianqiu Chen, Jie Ren, Chaofeng Zhang & Fei Ji. (2019) Palladium(II)-Catalyzed Efficient Synthesis of Wedelolactone and Evaluation as Potential Tyrosinase Inhibitor. Molecules 24:22, pages 4130.
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Reddymasu Sireesha, Reddymasu Sreenivasulu, Choragudi Chandrasekhar & Mannam Subba Rao. (2019) A Facile, Efficient and Selective Deprotection of P - Methoxy Benzyl Ethers Using Zinc (II) Trifluoromethanesulfonate. Letters in Organic Chemistry 16:12, pages 955-958.
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Ryan E. Mewis & Stephen J. Archibald. (2019) Side-bridged cyclam transition metal complexes bearing a phenolic ether or a phenolate pendent arm. Polyhedron 171, pages 578-589.
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Genevieve H. Dennison, Jonathan M. White & Martin R. Johnston. (2016) Efficient access to Unsymmetrically 3-Substituted-1,10-Phenanthrolines via Microwave Assisted Friedländer Condensation with Aldehydes.. ChemistrySelect 1:20, pages 6434-6437.
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Nicolas Rival, Arantxa Albornoz Grados, Lucie Schiavo, Françoise Colobert & Gilles Hanquet. (2015) Mild deprotection of PMB ethers using tert-butyl bromide. Tetrahedron Letters 56:49, pages 6823-6826.
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Andivelu Ilangovan, Karnambaram Anandhan & Mahabir Prasad Kaushik. (2015) Facile and selective deprotection of PMB ethers and esters using oxalyl chloride. Tetrahedron Letters 56:9, pages 1080-1084.
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. 2014. Greene's Protective Groups in Organic Synthesis. Greene's Protective Groups in Organic Synthesis 472 553 .
. 2014. Greene's Protective Groups in Organic Synthesis. Greene's Protective Groups in Organic Synthesis 17 471 .
Michael E. Jung & Pierre Koch. (2011) Mild, selective deprotection of PMB ethers with triflic acid/1,3-dimethoxybenzene. Tetrahedron Letters 52:46, pages 6051-6054.
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Jun Xue, Vipin Kumar, Sirajud D. Khaja, E.V. Chandrasekaran, Robert D. Locke & Khushi L. Matta. (2009) Syntheses of fluorine-containing mucin core 2/core 6 structures using novel fluorinated glucosaminyl donors. Tetrahedron 65:40, pages 8325-8335.
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Min Li, Anmei Wu & Peijie Zhou. (2006) A concise synthesis of (+)-pancratistatin using pinitol as a chiral building block. Tetrahedron Letters 47:22, pages 3707-3710.
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Ch. Raji Reddy, Amar G. Chittiboyina, Rajashaker Kache, Jae-Chul Jung, E. Blake Watkins & Mitchell A. Avery. (2005) The trimethylsilyl xylyl (TIX) ether: a useful protecting group for alcohols. Tetrahedron 61:5, pages 1289-1295.
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Ling Ma, Jessica C. Morgan, Wendy E. Stancill & William E. Allen. (2004) Phosphorylated 1,6-diphenyl-1,3,5-hexatriene. Bioorganic & Medicinal Chemistry Letters 14:5, pages 1075-1078.
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Gangavaram V. Madhava Sharma, Ch Govardhan Reddy & Palakodety Radha Krishna. (2003) Zirconium(IV) Chloride Catalyzed New and Efficient Protocol for the Selective Cleavage of p -Methoxybenzyl Ethers . The Journal of Organic Chemistry 68:11, pages 4574-4575.
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Ronald J. Hinklin & Laura L. Kiessling. (2002) p -Methoxybenzyl Ether Cleavage by Polymer-Supported Sulfonamides . Organic Letters 4:7, pages 1131-1133.
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Jie Xia, Saeed A Abbas, Robert D Locke, Conrad F Piskorz, James L Alderfer & Khushi L Matta. (2000) Use of 1,2-dichloro 4,5-dicyanoquinone (DDQ) for cleavage of the 2-naphthylmethyl (NAP) group. Tetrahedron Letters 41:2, pages 169-173.
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J.S Yadav, H.M Meshram, G Sudershan Reddy & G Sumithra. (1998) Microwave thermolysis IV: Selective deprotection of MPM ethers using clay supported ammonium nitrate “clayan” in dry media. Tetrahedron Letters 39:19, pages 3043-3046.
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K. J. HODGETTS & T. W. WALLACE. (2010) ChemInform Abstract: Cleavage or Acetyl‐de‐Alkylation of 4‐Methoxybenzyl (MPM) Ethers Using Acetic Acid.. ChemInform 25:43.
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