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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 10
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Original Articles

An Improved Synthesis of 5,7-Dimethoxy-4-methylphthalide, A Key Intermediate in the Synthesis of Mycophenolic Acid

Gergely M. Makara Department of Medicinal Chemistry, School of Pharmacy, State University of New York at Buffalo, Buffalo, NY, 14260
,
Kevin Klubek Department of Medicinal Chemistry, School of Pharmacy, State University of New York at Buffalo, Buffalo, NY, 14260
&
Wayne K. Anderson Department of Medicinal Chemistry, School of Pharmacy, State University of New York at Buffalo, Buffalo, NY, 14260
Pages 1935-1942 | Received 15 Nov 1995, Published online: 21 Aug 2006

Citations (11)

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Read on this site (2)

Rogelio Jiménez, Luís A. Maldonado & Héctor Salgado-Zamora. (2010) Synthesis of demethylated nidulol via an intramolecular Michael reaction. Natural Product Research 24:13, pages 1274-1281.
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Adrián Covarrubias-Zúnniga, José Diaz-Dominguez & José S. Olguín-Uribe. (2001) SYNTHESIS OF 6-ALLYL-7-HYDROXY-5-METHOXY-4-METHYLPHTHALIDE, A KEY INTERMEDIATE IN THE SYNTHESIS OF MYCOPHENOLIC ACID. Synthetic Communications 31:9, pages 1373-1381.
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Articles from other publishers (9)

Shuang Chen, Yingying Xin & Chen Zhao. (2021) Multispectroscopic Analysis in the Synthesis of Lignin-Based Biophenolic Resins. ACS Sustainable Chemistry & Engineering 9:46, pages 15653-15660.
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Zhiwen Gao, Xueling Lang, Shuang Chen & Chen Zhao. (2021) Mini-Review on the Synthesis of Lignin-Based Phenolic Resin. Energy & Fuels 35:22, pages 18385-18395.
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Peter Angehrn, Stefan Buchmann, Christoph Funk, Erwin Goetschi, Hans Gmuender, Paul Hebeisen, Dirk Kostrewa, Helmut Link, Thomas Luebbers, Raffaello Masciadri, Joergen Nielsen, Peter Reindl, Fabienne Ricklin, Anne Schmitt-Hoffmann & Frank-Peter Theil. (2004) New Antibacterial Agents Derived from the DNA Gyrase Inhibitor Cyclothialidine. Journal of Medicinal Chemistry 47:6, pages 1487-1513.
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Adrián Covarrubias-Zúñiga, Armando Gonzalez-Lucas & Mireya M. Domı́nguez. (2003) Total synthesis of mycophenolic acid. Tetrahedron 59:11, pages 1989-1994.
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Robert M. Garbaccio, Shawn J. Stachel, Daniel K. Baeschlin & Samuel J. Danishefsky. (2001) Concise Asymmetric Syntheses of Radicicol and Monocillin I. Journal of the American Chemical Society 123:44, pages 10903-10908.
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Youngmin Lee, Yasunari Fujiwara, Katsuji Ujita, Miki Nagatomo, Hiroshi Ohta & Isao Shimizu. (2001) Syntheses of Mycophenolic Acid and Its Analogs by Palladium Methodology. Bulletin of the Chemical Society of Japan 74:8, pages 1437-1443.
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Robert M. Garbaccio & Samuel J. Danishefsky. (2000) Efficient Asymmetric Synthesis of Radicicol Dimethyl Ether:  A Novel Application of Ring-Forming Olefin Metathesis. Organic Letters 2:20, pages 3127-3129.
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Madhusudan V. Paradkar, Sanjeev A. Kulkarni, Augustine R. Joseph & Anup A. Ranade. (2019) An Efficient synthesis of Dimethoxyphthalides. Journal of Chemical Research 2000:8, pages 364-366.
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G. M. MAKARA, K. KLUBEK & W. K. ANDERSON. (2010) ChemInform Abstract: An Improved Synthesis of 5,7‐Dimethoxy‐4‐methylphthalide, a Key Intermediate in the Synthesis of Mycophenolic Acid.. ChemInform 27:34.
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