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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 1
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Original Articles

A New Versatile Synthesis of N,N′,N″,N″′-Tetra-(2-carboxyethyl)-and N,N′,N″,N″′-Tetra-(3-aminopropyl)-tetraazacycloalkanes by Michael Addition of Polyazacycloalkanes to Acrylic Acid and Acrylonitrile

C. Gros Laboratoire d'Ingénierie Moléculaire pour la Séparation et les Applications des Gaz (L.I.M.S.A.G.), U.M.R. n° 9953, Université de Bourgogne, Faculté des Sciences Gabriel, 21100, Dijon, France
,
H. Chollet Commissariat à l'Energie Atomique (C.E.A.), Centre d'Etudes de Valduc, 21120, Is-Sur-Tille, France; Laboratoire de Synthèse et d'Electrosynthèse Organométalliques, U.R.A. 1685, Université de Bourgogne, Faculté des Sciences Gabriel, 21100, Dijon, France
,
A. K. Mishra Laboratoire d'Ingénierie Moléculaire pour la Séparation et les Applications des Gaz (L.I.M.S.A.G.), U.M.R. n° 9953, Université de Bourgogne, Faculté des Sciences Gabriel, 21100, Dijon, France
&
R. Guilard Laboratoire d'Ingénierie Moléculaire pour la Séparation et les Applications des Gaz (L.I.M.S.A.G.), U.M.R. n° 9953, Université de Bourgogne, Faculté des Sciences Gabriel, 21100, Dijon, France
Pages 35-47 | Received 16 May 1995, Published online: 21 Aug 2006

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B. Jebasingh & V. Alexander. (2004) Efficient Reduction of tetrakis(2‐Cyanoethyl)cyclen with Sodium–Toluene and Synthesis of Carboxymethyl‐ and Hydroxyethyl Functionalized Second Generation Pendant Arms Appended Cyclens. Synthetic Communications 34:15, pages 2843-2848.
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Articles from other publishers (12)

Mathias Gressenbuch, Ulrike Lehmann & Berthold Kersting. (2016) Synthesis and structural chemistry of bicyclic hexaaza-dithia macrocycles containing pendant donor groups. New Journal of Chemistry 40:7, pages 5731-5739.
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Augustin de Castries, Aude Escande, Hélène Fensterbank, Emmanuel Magnier, Jérôme Marrot & Chantal Larpent. (2007) Synthesis of N-tetrasubstituted cyclam derivatives appended with sulfonyl or sulfinyl groups via aza-Michael addition. Tetrahedron 63:41, pages 10330-10336.
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Katie J. Heroux, Katrina S. Woodin, David J. Tranchemontagne, Peter C. B. Widger, Evan Southwick, Edward H. Wong, Gary R. Weisman, Sterling A. Tomellini, Thaddeus J. Wadas, Carolyn J. Anderson, Scott Kassel, James A. Golen & Arnold L. Rheingold. (2007) The long and short of it: the influence of N-carboxyethyl versusN-carboxymethyl pendant arms on in vitro and in vivo behavior of copper complexes of cross-bridged tetraamine macrocycles. Dalton Transactions:21, pages 2150.
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Joseph S. AmatoJohn Y. L. ChungRaymond J. CvetovichRobert A. ReamerDalian ZhaoGeorge ZhouXiaoyi Gong. (2004) Acrylate as an Efficient Dimethylamine Trap for the Practical Synthesis of 1- tert -Butyl-4-piperidone via Transamination . Organic Process Research & Development 8:6, pages 939-941.
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N.F. Curtis. 2003. Comprehensive Coordination Chemistry II. Comprehensive Coordination Chemistry II 447 474 .
Deyuan Kong & Yuyuan Xie. (2002) Synthesis, structural characterization of tetraazamacrocyclic ligand, five-coordinated zinc(II) complex. Inorganica Chimica Acta 338, pages 142-148.
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De-Yuan Kong & Yu-Yuan Xie. (2000) Synthesis, structural characterization and potentiometric studies of divalent metal complexes with an octadentate tetraazamacrocyclic ligand and their DNA cleavage ability. Polyhedron 19:12, pages 1527-1537.
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Deyuan Kong, Chen Qin, Linhua Meng & Yuyuan Xie. (1999) Synthesis, structural characterization and antitumor activity evaluations of copper complex with tetraazamacrocyclic ligand. Bioorganic & Medicinal Chemistry Letters 9:8, pages 1087-1092.
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Béatrice Gaudinet-Hamann, Jiarong Zhu, Hélène Fensterbank & Chantal Larpent. (1999) A convenient synthesis of bis-tetraazamacrocycles. Tetrahedron Letters 40:2, pages 287-290.
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Liu Yong, Xue Guo‐Ping & Wu Cheng‐Tai. (2010) Synthesis of novel N ‐aminoethyl cyclic polyamines . Chinese Journal of Chemistry 16:5, pages 448-451.
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Liu Yong, Xue Guo‐Ping, Wu Cheng‐Tai & Luo Bao‐Sheng. (2010) Synthesis and crystal structure of a Ni(II) complex with 1,7‐diaminoethyl‐4,10‐dimethyl‐1,4,7,10‐tetraazacyclododecane. Chinese Journal of Chemistry 16:1, pages 16-21.
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C. GROS, H. CHOLLET, A. K. MISHRA & R. GUILARD. (2010) ChemInform Abstract: A New Versatile Synthesis of N,N′,N′′,N′′′‐Tetra(2‐carboxyethyl)‐ and N,N′,N′′,N′′′‐Tetra(3‐aminopropyl)‐tetraazacycloalkanes by Michael Addition of Polyazacycloalkanes to Acrylic Acid and Acrylonitrile.. ChemInform 27:22.
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