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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 8
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Original Articles

A New Method for the Reductive Cleavage of S-S Bond by the System of Cp2TiCl2/i-BuMgBr/THF and its Application in Synthesis of α-Alkylthio Carbonyl Compounds

Xian Huang Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
&
Wei-Xin Zheng Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
Pages 1297-1301 | Received 06 Oct 1998, Published online: 17 Sep 2007

Citations (16)

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Weihui Zhong, Xiaoyuan Chen & Yongmin Zhang. (2000) Low-valent Titanium Induced Simultaneous Reduction of Nitro Group and S-S Bond in Nitrodisulfides: A Novel Method For the Synthesis of Benzothiazoline, Benzothiazoles and 2,3-Dihydro- 1,5-benzothiazepines. Synthetic Communications 30:24, pages 4451-4460.
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Xian Huang & Wei-Xin Zheng. (2000) A New Path for the Reductive Cleavage of Te-Te Bond by the System of Cp2TiCl2/i-BuMgBr and ITS Utility in Synthesis of Unsymmetrical Tellurides. Synthetic Communications 30:8, pages 1365-1369.
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Articles from other publishers (14)

Jèssica Margalef & Joseph S. M. Samec. (2020) Assessing Methodologies to Synthesize α‐Sulfenylated Carbonyl Compounds by Green Chemistry Metrics. ChemSusChem 14:3, pages 808-823.
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Lingxiao Wang, Jie Qiao, Jiancong Wei, Zhiwu Liang, Xinhua Xu & Ningbo Li. (2020) Air-stable binuclear Titanium(IV) salophen perfluorobutanesulfonate with zinc power catalytic system and its application to C–S and C–Se bond formation. Tetrahedron 76:4, pages 130750.
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Qian Chen, Yulin Huang, Xiaofeng Wang, Chunxiao Wen, Xinxing Yan & Jiekun Zeng. (2017) Cs2CO3-promoted carbon–sulfur bond construction via cross dehydrogenative coupling of thiophenols with acetonitrile. Tetrahedron Letters 58:41, pages 3928-3931.
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Qian Chen, Xiaofeng Wang, Chunxiao Wen, Yulin Huang, Xinxing Yan & Jiekun Zeng. (2017) Cs 2 CO 3 -promoted cross-dehydrogenative coupling of thiophenols with active methylene compounds . RSC Advances 7:63, pages 39758-39761.
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Yogesh Siddaraju & Kandikere Ramaiah Prabhu. (2016) Iodine Promoted Regioselective α-Sulfenylation of Carbonyl Compounds using Dimethyl Sulfoxide as an Oxidant. Organic Letters 18:23, pages 6090-6093.
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Yi-Wei Liu, Satpal Singh Badsara, Yi-Chen Liu & Chin-Fa Lee. (2015) K 2 S 2 O 8 /I 2 promoted syntheses of α-thio-β-dicarbonyl compounds via oxidative C–S coupling reactions under transition metal-free and solvent-free conditions . RSC Advances 5:55, pages 44299-44305.
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Liang‐Hua Zou, Daniel L. Priebbenow, Long Wang, Jakob Mottweiler & Carsten Bolm. (2013) Copper‐Catalyzed Synthesis of α‐Thioaryl Carbonyl Compounds Through SS and CC Bond Cleavage. Advanced Synthesis & Catalysis 355:13, pages 2558-2563.
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Catherine A. Campos & Brandon L. Ashfeld. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
Ebrahim Kianmehr, Mansoureh Mirza Agha & Hamid Estiri. (2010) Reaction of ammonium ylides with alkyl thiocyanates in aqueous and non-aqueous media. Monatshefte für Chemie - Chemical Monthly 141:4, pages 409-411.
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Xiao Bo Xu, Xian Hong Yin, Yu Yang Zhu, Xin Hua Xu, Tao Luo, Yin Hui Li, Xiong Lu, Ling Ling Shao, Jian Gao Pan & Rong Hua Yang. (2009) Reduction cleavage of S–S bond by Zn/Cp 2 TiCl 2 : Application for the synthesis of β-arylthiocarbonyl compounds . Journal of Chemical Research 2009:12, pages 750-752.
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I. V. Koval’. (2005) Synthesis, Structure, and Physicochemical Characteristics of Thiols. Russian Journal of Organic Chemistry 41:5, pages 631-648.
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I. Shcherbakova & A.F. Pozharskii. 2005. Comprehensive Organic Functional Group Transformations II. Comprehensive Organic Functional Group Transformations II 89 235 .
Michael B. Smith. 2003. Compendium of Organic Synthetic Methods. Compendium of Organic Synthetic Methods 483 708 .
Xian Huang & Wei‐Xin Zheng. (2010) ChemInform Abstract: A New Method for the Reductive Cleavage of S—S Bond by the System of Cp 2 TiCl 2 /i‐BuMgBr/THF and Its Application in Synthesis of α‐Alkylthio Carbonyl Compounds. . ChemInform 30:28.
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