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Journal of Coordination Chemistry Volume 62, 2009 - Issue 21
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Original Articles

Synthesis and characterization of Cu(II) and Ni(II) complexes of some 4-bromo- N -(di(alkyl/aryl)carbamothioyl) benzamide derivatives

Gün Binzet Department of Chemistry, Faculty of Arts and Science, Mersin University, Mersin, TR-33343, Turkey
,
Nevzat Külcü Department of Chemistry, Faculty of Arts and Science, Mersin University, Mersin, TR-33343, Turkey
,
Ulrich Flörke Department of Chemistry, University of Paderborn, Paderborn, D-33098, Germany
&
Hakan Arslan Department of Chemistry, Faculty of Pharmacy, Mersin University, Mersin, TR-33169, Turkey; Department of Natural Sciences, Fayetteville State University, Fayetteville, NC-28301, USACorrespondence[email protected]
Pages 3454-3462 | Received 25 Feb 2009, Accepted 10 Apr 2009, Published online: 22 Sep 2010

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Lathewdeipor Shadap, Venkanna Banothu, Uma Adepally, Sanjay Adhikari & Mohan Rao Kollipara. (2020) Variable structural bonding modes and antibacterial studies of thiosemicarbazone ligands of ruthenium, rhodium, and iridium metal complexes. Journal of Coordination Chemistry 73:1, pages 175-187.
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Sohail Saeed & Rizwan Hussain. (2014) Preparation and characterization of copper sulfide nanoparticles from symmetrical [(Bu)2NC(S)NC(O)C6H3(3,5-NO2)2]2Cu(II) and [(Bu)2NC(S)NC(O)C6H4(4-NO2)]2Cu(II) complexes by thermolysis. Journal of Coordination Chemistry 67:17, pages 2942-2953.
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Aamer Saeed, Ulrich Flörke & Mauricio F. Erben. (2014) A review on the chemistry, coordination, structure and biological properties of 1-(acyl/aroyl)-3-(substituted) thioureas. Journal of Sulfur Chemistry 35:3, pages 318-355.
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Sohail Saeed, Naghmana Rashid, Mohammad Azad Malik, Paul O’Brien & Wing-Tak Wong. (2013) Nickel(II) complexes of N-(dialkylcarbamothioyl)-4-nitrobenzamide as single-source precursors for the deposition of nanostructured nickel sulfide thin films by chemical vapor deposition. Journal of Coordination Chemistry 66:16, pages 2788-2801.
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Sohail Saeed, Naghmana Rashid, Rizwan Hussain, Jerry P. Jasinski, Amanda C. Keeley & Sajid Khan. (2013) Nanoparticles and nanocrystals of a new bidentate nickel(II) complex of N-[ethyl(propan-2-yl)carbamothioyl]-4-nitrobenzamide: synthesis, characterization, and crystal structures. Journal of Coordination Chemistry 66:1, pages 126-138.
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Hiram Pérez, B. O’Reilly, A.M. Plutín, R. Martínez, R. Durán, I.G. Collado & Y.P. Mascarenhas. (2011) Synthesis, characterization, and crystal structure of Ni(II) and Cu(II) complexes with N-furoyl-N′,N′-diethylthiourea: antifungal activity. Journal of Coordination Chemistry 64:16, pages 2890-2898.
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N. Gunasekaran, N. Remya, S. Radhakrishnan & R. Karvembu. (2011) Ruthenium(II) carbonyl complexes with N-[di(alkyl/aryl)carbamothioyl]benzamide derivatives and triphenylphosphine as effective catalysts for oxidation of alcohols. Journal of Coordination Chemistry 64:3, pages 491-501.
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Articles from other publishers (38)

Charlestine Soh, Mohan Rao Kollipara, Danny F Diengdoh, Venkanna Banothu, Werner Kaminsky & E.K. Rymmai. (2022) Cyclopentadienyl and indenyl ruthenium(II) complexes containing pyridyl/pyrimidyl based thiourea derivative ligands: Syntheses, antibacterial and antioxidant studies. Journal of Molecular Structure 1269, pages 133751.
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Ebube E. Oyeka, Ilknur Babahan, Bernard Eboma, Kenechukwu J. Ifeanyieze, Obinna C. Okpareke, Esin P. Coban, Ali Özmen, Burak Coban, Mehran Aksel, Namık Özdemir, Tatiana.V. Groutso, Jude I. Ayogu, Ufuk Yildiz, Mehmet Dinçer Bilgin, H. Halil Biyik, Briana R. Schrage, Christopher J. Ziegler & Jonnie N. Asegbeloyin. (2021) Biologically active acylthioureas and their Ni(II) and Cu(II) Complexes: Structural, spectroscopic, anti-proliferative, nucleolytic and antimicrobial studies. Inorganica Chimica Acta 528, pages 120590.
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Muhammad Ashfaq, Muhammad Nawaz Tahir, Shabbir Muhammad, Khurram Shahzad Munawar, Akbar Ali, Georgii Bogdanov & Saleh S. Alarfaji. (2021) Single-Crystal Investigation, Hirshfeld Surface Analysis, and DFT Study of Third-Order NLO Properties of Unsymmetrical Acyl Thiourea Derivatives. ACS Omega 6:46, pages 31211-31225.
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Sidra Akhter, Saeed Ullah, Sammer Yousuf, Atia-tul-Wahab, Hina Siddiqui & M. Iqbal Choudhary. (2021) Synthesis, crystal structure and Hirshfeld Surface analysis of benzamide derivatives of thiourea as potent inhibitors of α-glucosidase in-vitro. Bioorganic Chemistry 107, pages 104531.
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Lan‐Xin Peng, Dan Wang, De‐Xiang Zhang, Zhi‐Jiao Zhang, Qi Zhou, Hai‐Pu Li & Ying Yang. (2020) Synthesis and Characterization of Copper(I) Halide Complexes Prepared with Bipodal Diacylthioureas. European Journal of Inorganic Chemistry 2020:26, pages 2521-2529.
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Xiaopei Li, Yongjie Zhang & Yizhuang Xu. (2020) Modified asynchronous orthogonal sample design scheme @ Job’s method to determine the stoichiometric ratio in the molecular association system. Journal of Molecular Structure 1206, pages 127757.
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Duraid H. Al-Amily & Mohammed Hassan Mohammed. (2019) Design, Synthesis, and Docking Study of Acyl Thiourea Derivatives as Possible Histone Deacetylase Inhibitors with a Novel Zinc Binding Group. Scientia Pharmaceutica 87:4, pages 28.
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Lathewdeipor Shadap, Siewdorlang Diamai, Jaya Lakshmi Tyagi, Krishna Mohan Poluri, Werner Kaminsky & Mohan Rao Kollipara. (2019) Synthesis, biological evaluation and colorimetric sensing studies of platinum group metal complexes comprising pyrazine based thiourea derivatives. Journal of Organometallic Chemistry 897, pages 207-216.
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Jonnie N. Asegbeloyin, Kenechukwu J. Ifeanyieze, Obinna C. Okpareke, Ebube E. Oyeka & Tatiana V. Groutso. (2019) Crystal structure and Hirshfeld surface analysis of a new dithioglycoluril: 1,4-bis(4-methoxyphenyl)-3 a -methyltetrahydroimidazo[4,5- d ]imidazole-2,5(1 H ,3 H )-dithione . Acta Crystallographica Section E Crystallographic Communications 75:9, pages 1297-1300.
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Sunil K. Pandey, Durga P. Singh, Seema Pratap, Gaetano Marverti & R.J. Butcher. (2019) Copper(I) complexes of N-(2/4 methoxy/2-chloro-4-nitro)phenyl-N′ (methoxycarbonyl)thiocarbamides as potential anticancer agents: Synthesis, crystal structure, in vitro cytotoxicity and DNA damage studies. Polyhedron 170, pages 431-439.
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Lathewdeipor Shadap, Siewdorlang Diamai, Venkanna Banothu, D.P.S. Negi, Uma Adepally, Werner Kaminsky & Mohan Rao Kollipara. (2019) Half sandwich platinum group metal complexes of thiourea derivative ligands with benzothiazole moiety possessing anti-bacterial activity and colorimetric sensing: Synthesis and characterisation. Journal of Organometallic Chemistry 884, pages 44-54.
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Ebube Evaristus Oyeka, Jonnie Niyi Asegbeloyin, Ilknur Babahan, Bernard Eboma, Obinna Okpareke, Joseph Lane, Akachukwu Ibezim, H. Halil Bıyık, Bahadır Törün & David Chukwuma Izuogu. (2018) Synthesis, crystal structure, computational analysis and biological properties of 1-(4-chlorobenzoyl)-3-[2-(2-{2-[3-(4-chlorobenzoyl)-thioureido]-ethoxy}ethoxy)ethyl]-thiourea and its Ni(II) and Cu(II) complexes. Journal of Molecular Structure 1168, pages 153-164.
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Ibaniewkor L. Mawnai, Sanjay Adhikari, Werner Kaminsky & Mohan Rao Kollipara. (2018) Synthesis of strained complexes of arene d6 metals with benzoylthiourea and their spectral studies. Journal of Organometallic Chemistry 869, pages 26-36.
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Xianhui Hou, Fanfan Wang, Li Han, Xia Pan, Haipu Li, Ying Yang & Herbert W. Roesky. (2018) Self-Assembly of Discrete Copper(I)-Halide Complexes with Diacylthioureas. Zeitschrift für anorganische und allgemeine Chemie 644:3, pages 142-148.
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Gun Binzet, Ersan Turunc, Ulrich Flörke, Nevzat Külcü & Hakan Arslan. (2018) Crystal Structure and Cyclic Voltammetric Studies on the Metal Complexes of N -(Dimethylcarbamothioyl)-4-fluorobenzamide . Journal of Chemistry 2018, pages 1-8.
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Dan Wang, Su‐Yun Wu, Hai‐Pu Li, Ying Yang & Herbert W. Roesky. (2017) Synthesis and Characterization of Copper Complexes with the N ‐(2,6‐Diisopropylphenyl)‐ N′ ‐acylthiourea Ligands . European Journal of Inorganic Chemistry 2017:10, pages 1406-1413.
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N. Gunasekaran, N.S.P. Bhuvanesh & R. Karvembu. (2017) Synthesis, characterization and catalytic oxidation property of copper(I) complexes containing monodentate acylthiourea ligands and triphenylphosphine. Polyhedron 122, pages 39-45.
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Ilkay Gumus, Ummuhan Solmaz, Omer Celik, Gun Binzet, Gulten Kavak Balcı & Hakan Arslan. (2015) Synthesis, characterization and crystal structure of cis-bis[4-fluoro-N-(diethylcarbamothioyl)benzamido-κ2O,S]platinum(II). European Journal of Chemistry 6:3, pages 237-241.
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Mannar R. Maurya, Bhawna Uprety, Fernando Avecilla, Saba Tariq & Amir Azam. (2015) Palladium(II) complexes of OS donor N-(di(butyl/phenyl)carbamothioyl)benzamide and their antiamoebic activity. European Journal of Medicinal Chemistry 98, pages 54-60.
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Su‐Yun Wu, Xiao‐Ya Zhao, Hai‐Pu Li, Ying Yang & Herbert W. Roesky. (2015) Synthesis and Characterization of N , N ‐Di‐substituted Acylthiourea Copper(II) Complexes . Zeitschrift für anorganische und allgemeine Chemie 641:5, pages 883-889.
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Kumaramangalam Jeyalakshmi, Yuvaraj Arun, Nattamai S. P. Bhuvanesh, Paramasivan Thirumalai Perumal, Anandaram Sreekanth & Ramasamy Karvembu. (2015) DNA/protein binding, DNA cleavage, cytotoxicity, superoxide radical scavenging and molecular docking studies of copper( ii ) complexes containing N-benzyl-N′-aryl-N′′-benzoylguanidine ligands . Inorganic Chemistry Frontiers 2:8, pages 780-798.
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Sohail Saeed, Khuram Shahzad Ahmed, Naghmana Rashid, Mohammad Azad Malik, Paul O’Brien, Masood Akhtar, Rizwan Hussain & Wing-Tak Wong. (2015) Symmetrical and unsymmetrical nickel(II) complexes of N-(dialkylcarbamothioyl)-nitro substituted benzamide as single-source precursors for deposition of nickel sulfide nanostructured thin films by AACVD. Polyhedron 85, pages 267-274.
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F. Aydin, D. Aykaç, N. Burcu Arslan & C. Kazak. (2014) Synthesis, characterization, and crystal structure of bis[4-(3′-benzoyl)thiocarbamidophenyl]ether. Crystallography Reports 59:7, pages 955-960.
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N. Selvakumaran, N.S.P. Bhuvanesh, A. Endo & R. Karvembu. (2014) Synthesis, structure, DNA and protein binding studies, and cytotoxic activity of nickel(II) complexes containing 3,3-dialkyl/aryl-1-(2,4-dichlorobenzoyl)thiourea ligands. Polyhedron 75, pages 95-109.
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Gün Binzet, Gülten Kavak, Nevzat Külcü, Süheyla Özbey, Ulrich Flörke & Hakan Arslan. (2013) Synthesis and Characterization of Novel Thiourea Derivatives and Their Nickel and Copper Complexes. Journal of Chemistry 2013, pages 1-9.
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Gun Binzet, Bülent Zeybek, Esma Kılıç, Nevzat Külcü & Hakan Arslan. (2013) Determination of the Ionization Constants of Some Benzoyl Thiourea Derivatives in Dioxane-Water Mixture. Journal of Chemistry 2013, pages 1-7.
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H. Pérez, R. S. Corrêa, B. O’Reilly, A. M. Plutín, C. C. P. Silva & Y. P. Mascarenhas. (2012) Spectroscopic characterization and crystal structure of cis-Bis(N-(2-benzoyl)-N′,N′-diphenylthioureato-k 2O,S)nickel(II). Journal of Structural Chemistry 53:5, pages 921-926.
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Gun Binzet, Ulrich Flörke, Nevzat Külcü & Hakan Arslan. (2012) Crystal and molecular structure of bis(4-bromo-N-(di-n-butylcarbamothioyl)benzamido) copper(II) complex. European Journal of Chemistry 3:2, pages 211-213.
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Gun Binzet, Ulrich Flörke, Nevzat Külcü & Hakan Arslan. (2012) Crystal and molecular structure of bis(4-bromo-N-(diethylcarbamothioyl)benzamido)nickel(II) complex. European Journal of Chemistry 3:1, pages 37-39.
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N. Gunasekaran, S.W. Ng, E.R.T. Tiekink & R. Karvembu. (2012) Hypodentate coordination of N,N-di(alkyl/aryl)-N′-acylthiourea derivatives in Cu(I) complexes. Polyhedron 34:1, pages 41-45.
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N. Gunasekaran, P. Jerome, Seik Weng Ng, Edward R.T. Tiekink & R. Karvembu. (2012) Tris-chelate complexes of cobalt(III) with N-[di(alkyl/aryl)carbamothioyl] benzamide derivatives: Synthesis, crystallography and catalytic activity in TBHP oxidation of alcohols. Journal of Molecular Catalysis A: Chemical 353-354, pages 156-162.
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Hiram Pérez, Rodrigo S. Corrêa, Ana María Plutín, Beatriz O'Reilly & Marcelo B. Andrade. (2011) Probing the relationships between molecular conformation and intermolecular contacts in N , N -dibenzyl- N ′-(furan-2-carbonyl)thiourea . Acta Crystallographica Section C Crystal Structure Communications 68:1, pages o19-o22.
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Paniz Tashakkori, Serap Seyhan Bozkurt, Melek Merdivan, Gun Binzet & Nevzat Kulcu. (2012) Separation and preconcentration of palladium using benzoylthiourea immobilized on a cationic surfactant coated silica gel. Analytical Methods 4:12, pages 4135.
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Gün Binzet, Ulrich Flörke, Nevzat Külcü & Hakan Arslan. (2011) cis -Bis[ N ′-(4-bromobenzoyl)- N , N -dimethylthioureato-κ 2 O , S ]copper(II) . Acta Crystallographica Section E Structure Reports Online 67:5, pages m648-m649.
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N. Selvakumaran, R. Karvembu, Seik Weng Ng & Edward R. T. Tiekink. (2011) 1-Benzoyl-3,3-bis(2-methylpropyl)thiourea. Acta Crystallographica Section E Structure Reports Online 67:3, pages o602-o602.
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Nanjappan Gunasekaran, Pandian Ramesh, Mondikalipudur Nanjappa Gounder Ponnuswamy & Ramasamy Karvembu. (2011) Monodentate coordination of N-[di(phenyl/ethyl)carbamothioyl]benzamide ligands: synthesis, crystal structure and catalytic oxidation property of Cu(i) complexes. Dalton Transactions 40:46, pages 12519.
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N. Gunasekaran, R. Karvembu, Seik Weng Ng & Edward R. T. Tiekink. (2010) 1-Benzoyl-3,3-dibutylthiourea. Acta Crystallographica Section E Structure Reports Online 66:10, pages o2601-o2601.
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N. Gunasekaran & R. Karvembu. (2010) Synthesis, characterization, and catalytic applications of Ru(III) complexes containing N-[di(alkyl/aryl)carbamothioyl]benzamide derivatives and triphenylphosphine/triphenylarsine. Inorganic Chemistry Communications 13:8, pages 952-955.
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