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Original Articles

A comparison of X-ray (STEM) and Auger electron spectroscopy for the microanalysis of grain boundary segregation

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Pages 759-768 | Received 02 Feb 1978, Published online: 27 Sep 2006

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W. Sigle, L.-S. Ciiang & W. Gusr. (2002) On the correlation between grain-boundary segregation, faceting and embrittlement in Bi-doped Cu. Philosophical Magazine A 82:8, pages 1595-1608.
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C.R. M. Grovenor, P.E. Batson, D.A. Smith & C. Wong. (1985) As segregation to grain boundaries in Si. Philosophical Magazine A 50:3, pages 409-423.
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P. Doig, D. Lonsdale & P. E. J. Flewitt. (1982) Segregation of embrittling elements to prior austenite grain boundaries in 2·25Cr–1 Mo steel. Metal Science 16:7, pages 335-344.
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P. Doig, D. Lonsdale & P.E. J. Flewitt. (1980) The spatial resolution of X-ray microanalysis in the scanning transmission electron microscope. Philosophical Magazine A 41:5, pages 761-775.
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Articles from other publishers (25)

C.-Y. Hsu, J. Stodolna, P. Todeschini, F. Delabrouille, V. Barnier, B. Radiguet & F. Christien. (2022) Solute interface segregation measurement: Cross comparison between four different analytical methods. Applied Surface Science 598, pages 153784.
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Chunfei Li, Masashi Watanabe, David W Ackland & David B Williams. (2003) Effect of rapid quenching on Sb grain-boundary segregation in Cu. Materials Letters 57:7, pages 1345-1350.
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V.J Keast & D.B Williams. (1999) Quantitative compositional mapping of Bi segregation to grain boundaries in Cu. Acta Materialia 47:15-16, pages 3999-4008.
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D. P. Schweinsberg, B. Sun, M. Cheng & H. Flitt. (1993) Potentiodynamic estimation of sensitization of 347 grade SS superheater tubes Part I: Effect of surface finish, scan rate and solution temperature. Journal of Applied Electrochemistry 23:11, pages 1097-1101.
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J.J. Hickey & J.H. Bulloch. (1992) Review of nondestructive techniques designed to evaluate elevated temperature toughness degradation. Theoretical and Applied Fracture Mechanics 18:1, pages 1-13.
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Anthony J. Garratt-Reed. (2020) Measurement of segregation at interfaces by AEM. Proceedings, annual meeting, Electron Microscopy Society of America 50:2, pages 1206-1207.
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Kishu HOSOITsunenobu YOKOSUKAToshimi YOSHIDAIsao MASAOKAYasuhiro SASADA. (1990) The Effect of P and Si Segregation to Grain Boundary on the Intergranular Corrosion of Type 304L Stainless Steel. Tetsu-to-Hagane 76:6, pages 948-955.
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D. B. Williams & A. D. RomigJr.Jr.. (2020) Measurement of solute segregation to grain boundaries in the AEM: A review. Proceedings, annual meeting, Electron Microscopy Society of America 46, pages 606-607.
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A. D. Romig, J. C. Lippold & M. J. Cieslak. (1988) An analytical electron microscope investigation of the phase transformations in a simulated heat-affected zone in alloy 800. Metallurgical Transactions A 19:1, pages 35-50.
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Mitsuru TANINO. (1984) Application of Modern Electron Microscopy to Ferrous Materials. Tetsu-to-Hagane 70:2, pages 158-165.
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P. Doig & P. E. J. Flewitt. (2011) The role of specimen and instrumental parameters in STEM‐EDS X‐ray microanalysis of thin foils. Journal of Microscopy 130:3, pages 377-388.
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T.J. SHAFFNER. 1983. Materials and Process Characterization. Materials and Process Characterization 497 527 .
P. Doig & P.E.J. Flewitt. (1983) STEM-EDS X-ray microanalysis of grain boundary segregations: The influence of electron probe size and grain boundary orientation. Micron and Microscopica Acta 14:3, pages 225-231.
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T. Malis & M. C. Chaturvedi. (2020) Variations in Grain Boundary Segregation for Al-8 Mg. Proceedings, annual meeting, Electron Microscopy Society of America 40, pages 626-627.
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P. Doig & P. E. J. Flewitt. (1982) The detection of monolayer grain boundary segregations in steels using stem-eds X-ray microanalysis. Metallurgical Transactions A 13:8, pages 1397-1403.
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C.R.M. Grovenor & C.M.F. Rae. (1981) A new method for observing the anisotropy of Bi segregation to Cu grain boundaries. Scripta Metallurgica 15:12, pages 1305-1308.
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P. Doig & P.E.J. Flewitt. (1981) Segregation of chromium to prior austenite boundaries during quenching of a %crl%mo steel. Acta Metallurgica 29:11, pages 1831-1841.
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Geoffrey C. Allen & Robert K. Wild. (1981) Analysis of grain boundary particles by scanning Auger microscopy. Applications of Surface Science 8:3, pages 278-289.
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P. Doig, D. Lonsdale & P. E. J. Flewitt. (1981) X-Ray microanalysis of grain boundary segregations in steels using the scanning transmission electron microscope. Metallurgical Transactions A 12:7, pages 1277-1282.
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J.K.L. Lai, D.J. Chastell & P.E.J. Flewitt. (1981) Precipitate phases in type 316 austenitic stainless steel resulting from long-term high temperature service. Materials Science and Engineering 49:1, pages 19-29.
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W. A. Straub & J. K. Hurwitz. (2002) Ferrous analysis. Analytical Chemistry 53:5, pages 44-61.
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P. Doig & P.E.J. Flewitt. (1980) The influence of microstructure on the localized corrosion behaviour of a 12%Cr1%Mo ferritic stainless steel. Materials Science and Engineering 43:1, pages 77-84.
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P.J. Goodhew & D. Chescoe. (1980) Microanalysis in the transmission electron microscope. Micron (1969) 11:2, pages 153-181.
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D. Lonsdale & P.E.J. Flewitt. (1979) The effect of small changes in impurity element content on the creep life of Cr1Mo steel. Materials Science and Engineering 41:1, pages 127-136.
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P. Doig, D. Lonsdale & P.E.J. Flewitt. (1979) Measurement of alloy and impurity elemental distributions in commercial steels using stem. Micron (1969) 10:4, pages 277-283.
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