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Food Additives & Contaminants: Part A Volume 26, 2009 - Issue 10
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Original Articles

Validation of a confirmatory analytical method for the determination of aflatoxins B1, B2, G1 and G2 in foods and feed materials by HPLC with on-line photochemical derivatization and fluorescence detection

Marilena Muscarella Istituto Zooprofilattico Sperimentale della Puglia e della Basilicata, Via Manfredonia 20, 71100 Foggia, Italy
,
Marco Iammarino Istituto Zooprofilattico Sperimentale della Puglia e della Basilicata, Via Manfredonia 20, 71100 Foggia, Italy
,
Donatella Nardiello Dipartimento di Scienze Agro-Ambientali, Chimica e Difesa Vegetale and BIOAGROMED, Università degli Studi di Foggia, Via Napoli 25, 71100 Foggia, Italy
,
Sonia Lo Magro Istituto Zooprofilattico Sperimentale della Puglia e della Basilicata, Via Manfredonia 20, 71100 Foggia, Italy
,
Carmen Palermo Dipartimento di Scienze Agro-Ambientali, Chimica e Difesa Vegetale and BIOAGROMED, Università degli Studi di Foggia, Via Napoli 25, 71100 Foggia, Italy
,
Diego Centonze Dipartimento di Scienze Agro-Ambientali, Chimica e Difesa Vegetale and BIOAGROMED, Università degli Studi di Foggia, Via Napoli 25, 71100 Foggia, ItalyCorrespondence[email protected]
&
Domenico Palermo Istituto Zooprofilattico Sperimentale della Puglia e della Basilicata, Via Manfredonia 20, 71100 Foggia, Italy
 show all
Pages 1402-1410 | Received 12 Oct 2008, Accepted 08 Jun 2009, Published online: 09 Sep 2009

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Baha’uddeen Salisu, Siti Marwanis Anua, Wan Ishak Wan Rosli, Nurzafirah Mazlan & Rosliza Haron. (2022) Ultra-fast RP-HPLC-FD-DAD for quantification of total aflatoxins in maize, rice, wheat, peanut and poultry feed without sample clean up, and population exposure risk assessment in Katsina, Nigeria: an optimization study. Journal of Environmental Science and Health, Part B 57:7, pages 541-553.
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Ali Heshmati, Amir Sasan Mozaffari Nejad & Fereshteh Mehri. (2021) Occurrence, dietary exposure, and risk assessment of aflatoxins in wheat flour from Iran. International Journal of Environmental Analytical Chemistry 0:0, pages 1-14.
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Jianrong Yang, Rui Zhao, Liting Song, Jungang Yin, Yanli You, Chengfeng Sun & Yanshen Li. (2017) Optimized Ultrasonic-Assisted Extraction of Aflatoxin B1 in Peanuts with Response Surface Methodology. Analytical Letters 50:4, pages 629-640.
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Ho Jin Kim, Mi Jin Lee, Hye Jin Kim, Soon Kil Cho, Hye Jin Park & Min Hee Jeong. (2017) Analytical method development and monitoring of Aflatoxin B1, B2, G1, G2 and Ochratoxin A in animal feed using HPLC with Fluorescence detector and photochemical reaction device. Cogent Food & Agriculture 3:1.
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Javed Iqbal, Muhammad Asif Asghar, Aftab Ahmed, Mobeen Ahmed Khan & Khalid Jamil. (2014) Aflatoxins contamination in Pakistani brown rice: a comparison of TLC, HPLC, LC–MS/MS and ELISA techniques. Toxicology Mechanisms and Methods 24:8, pages 544-551.
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Cheng Li, Gang Xie, Anxiang Lu, Hua Ping, Zhihong Ma, Yunxia Luan & Jihua Wang. (2014) Determination of Aflatoxins in Rice and Maize by Ultra-High Performance Liquid Chromatography–Tandem Mass Spectrometry with Accelerated Solvent Extraction and Solid-Phase Extraction. Analytical Letters 47:9, pages 1485-1499.
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Articles from other publishers (27)

Chammakalayil Sukumaran Arun, Pambayan Ulagan Mahalingam, Haris Parengal & Joby Thomas. (2023) Potential of Animal Excreta as a Source of Probiotic Lactic Acid Bacteria for Aflatoxin B1 Detoxification by the Surface Binding Mechanism. Journal of Pure and Applied Microbiology.
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Y Anastasia, R Maryam, R Widiastuti & Dalilah. (2023) Aflatoxins contamination in duck feedstuffs collected from Indramayu District. IOP Conference Series: Earth and Environmental Science 1253:1, pages 012130.
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Valeria Vita, Cinzia Franchino, Marco Iammarino & Rita De Pace. (2022) Aflatoxins contamination in nuts for direct human consumption: analytical findings from three years of official control in Italy. International Journal of Food Science & Technology 57:12, pages 7496-7504.
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Ying Liu, Yongpeng Jin, Qi Guo, Xiong Wang, Sunlin Luo, Wenjun Yang, Juntao Li & Yiqiang Chen. (2022) Immunoaffinity Cleanup and Isotope Dilution-Based Liquid Chromatography Tandem Mass Spectrometry for the Determination of Six Major Mycotoxins in Feed and Feedstuff. Toxins 14:9, pages 631.
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Nadeem Muhammad, Irshad Hussian, Amjad Ali, Tajamal Hussain, Azeem Intisar, Iftikhar Ul Haq, Qamar Subhani, Mateen Hedar, Jia-Lun Zhong, Muhammad Asif, Dandan Guo, Hairong Cui & Yan Zhu. (2022) A comprehensive review of liquid chromatography hyphenated to post-column photoinduced fluorescence detection system for determination of analytes. Arabian Journal of Chemistry 15:9, pages 104091.
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Manisha Dhanshetty, Pooja Thorat & Kaushik Banerjee. (2021) High-Throughput Analysis of Aflatoxins in Cereals, Nuts, and Processed Products Involving Automated Immunoaffinity Cleanup and Inline HPLC–Fluorescence Detection. Journal of AOAC INTERNATIONAL 104:6, pages 1526-1532.
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Julius Albert, Camilla A. More, Niklaus R. P. Dahlke, Zacharias Steinmetz, Gabriele E. Schaumann & Katherine Muñoz. (2021) Validation of a Simple and Reliable Method for the Determination of Aflatoxins in Soil and Food Matrices. ACS Omega 6:29, pages 18684-18693.
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Yunhong Huang, Fei Zhu, Jinhua Guan, Wei Wei & Long Zou. (2020) Label-Free Amperometric Immunosensor Based on Versatile Carbon Nanofibers Network Coupled with Au Nanoparticles for Aflatoxin B1 Detection. Biosensors 11:1, pages 5.
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K. Raksha Rao, A. V. Vipin & G. Venkateswaran. (2020) Molecular profile of non-aflatoxigenic phenotype in native strains of Aspergillus flavus. Archives of Microbiology 202:5, pages 1143-1155.
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Joseph Owuor Lalah, Solomon Omwoma & Dora A.O. Orony. 2020. Aflatoxin B1 Occurrence, Detection and Toxicological Effects. Aflatoxin B1 Occurrence, Detection and Toxicological Effects.
Jing Gao, Jing Wang, Chengxin Wu, Fujiang Hou, Shenghua Chang, Zhaofeng Wang, Qiaosheng Pu, Ding Guo & Hua Fu. (2018) Fast screening of aflatoxins in dairy cattle feeds with CE‐LIF method combined with preconcentration technique of vortex assisted low density solvent–microextraction. ELECTROPHORESIS 40:4, pages 499-507.
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Alex Paul Wacoo, Deborah Wendiro, Sarah Nanyonga, Joseph Hawumba, Wilbert Sybesma & Remco Kort. (2018) Feasibility of A Novel On-Site Detection Method for Aflatoxin in Maize Flour from Markets and Selected Households in Kampala, Uganda. Toxins 10:8, pages 327.
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Sasiprapa Choochuay, Jutamas Phakam, Prakorn Jala, Thanapoom Maneeboon & Natthasit Tansakul. (2018) Determination of Aflatoxin B 1 in Feedstuffs without Clean-Up Step by High-Performance Liquid Chromatography . International Journal of Analytical Chemistry 2018, pages 1-8.
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V. Vita, M. T. Clausi, C. Franchino & R. De Pace. (2016) Aflatoxin B1 contamination in feed from Puglia and Basilicata regions (Italy): 5 years monitoring data. Mycotoxin Research 32:4, pages 229-236.
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Muhammad Asif Asghar, Javed Iqbal, Aftab Ahmed, Mobeen Ahmed Khan, Zuzzer Ali Shamsuddin & Khalid Jamil. (2014) Development and validation of a high-performance liquid chromatography method with post-column derivatization for the detection of aflatoxins in cereals and grains. Toxicology and Industrial Health 32:6, pages 1122-1134.
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Zhi Liu, Hai-Long Wu, Hui-Wen Gu, Xiao-Li Yin, Li-Xia Xie, Yong Hu, Hui Xia, Shou-Xia Xiang & Ru-Qin Yu. (2016) Interference-free analysis of aflatoxin B 1 and G 1 in various foodstuffs using trilinear component modeling of excitation–emission matrix fluorescence data enhanced through photochemical derivatization . RSC Advances 6:31, pages 25850-25863.
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Natalia Arroyo-Manzanares, José F. Huertas-Pérez, Ana M. García-Campaña & Laura Gámiz-Gracia. (2015) Aflatoxins in animal feeds: A straightforward and cost-effective analytical method. Food Control 54, pages 74-78.
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Katarina Pavšič-Vrtač, Suvi Ojanperä, Juha Apajalahti, Karin Šrimpf & Gabrijela Tavčar-Kalcher. (2014) Analytical Procedures for the Determination of Aflatoxin B1 in Eggs of Laying Hens Using Immunoaffinity Columns and Liquid Chromatography with Post-Column Derivatisation and Fluorescence Detection. Food Analytical Methods 7:9, pages 1917-1924.
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A.M. Tavares, P. Alvito, S. Loureiro, H. Louro & M.J. Silva. (2013) Multi-mycotoxin determination in baby foods and in vitro combined cytotoxic effects of aflatoxin M 1 and ochratoxin A . World Mycotoxin Journal 6:4, pages 375-388.
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Constantinos K. Zacharis & Paraskevas D. Tzanavaras. (2013) Liquid chromatography coupled to on-line post column derivatization for the determination of organic compounds: A review on instrumentation and chemistries. Analytica Chimica Acta 798, pages 1-24.
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P. Rodrigues, A. Venâncio & N. Lima. (2012) Aflatoxigenic Fungi and Aflatoxins in Portuguese Almonds. The Scientific World Journal 2012, pages 1-9.
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G. Galaverna & C. Dall'Asta. 2012. Comprehensive Sampling and Sample Preparation. Comprehensive Sampling and Sample Preparation 381 403 .
María Ibáñez-Vea, Laura Ana Corcuera, Rebeca Remiro, María Teresa Murillo-Arbizu, Elena González-Peñas & Elena Lizarraga. (2011) Validation of a UHPLC-FLD method for the simultaneous quantification of aflatoxins, ochratoxin A and zearalenone in barley. Food Chemistry 127:1, pages 351-358.
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A. McDaniel, W.E. Holmes, K.L. Armbrust, D.L. Sparks & A. E. Brown. (2011) Effect of Matrix Clean-Up for Aflatoxin Analysis in Corn and Dried Distillers Grains. Natural Resources 02:04, pages 250-257.
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G. Shephard, F. Berthiller, P. Burdaspal, C. Crews, M. Jonker, R. Krska, S. MacDonald, B. Malone, C. Maragos, M. Sabino, M. Solfrizzo, H. van Egmond & T. Whitaker. (2011) Developments in mycotoxin analysis: an update for 2009-2010. World Mycotoxin Journal 4:1, pages 3-28.
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Marilena Muscarella, Marco Iammarino, Donatella Nardiello, Sonia Lo Magro, Carmen Palermo & Diego Centonze. 2011. Microbial Toxins. Microbial Toxins 203 210 .
C. Soares, P. Rodrigues, O. Freitas-Silva, L. Abrunhosa & A. Venâncio. (2010) HPLC method for simultaneous detection of aflatoxins and cyclopiazonic acid. World Mycotoxin Journal 3:3, pages 225-231.
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