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Enantiomer

A Journal of Sterochemistry

Volume 7, 2002 - Issue 4-5

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Original Articles

Comparison of CD Spectra of (2-Methylphenyl)- and (2,6-Dimethylphenyl)-phenylmethanols Leads to Erroneous Absolute Configurations

Masashi Kosaka Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, 980-8577, Japan

Shunsuke Kuwahara Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, 980-8577, Japan

Masataka Watanabe Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, 980-8577, Japan

Nobuyuki Harada Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba, Sendai, 980-8577, Japan

Gabriel E. Job School of Chemical Sciences, University of Illinois, 600 South Mathews Avenue, Urbana, IL, 61801, U.S.A

William H. Pirkle School of Chemical Sciences, University of Illinois, 600 South Mathews Avenue, Urbana, IL, 61801, U.S.A

Pages 213-217 | Published online: 17 Sep 2010

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https://doi.org/10.1080/10242430212878

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Gennaro Pescitelli. (2021) ECD exciton chirality method today: a modern tool for determining absolute configurations. Chirality 34:2, pages 333-363.
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Daniele Padula & Gennaro Pescitelli. (2018) How and How Much Molecular Conformation Affects Electronic Circular Dichroism: The Case of 1,1-Diarylcarbinols. Molecules 23:1, pages 128.
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Nobuyuki Harada. 2018. Chiral Analysis. Chiral Analysis 293 343 .

Daniele Padula, Javier Cerezo, Gennaro Pescitelli & Fabrizio Santoro. (2017) The shape of the electronic circular dichroism spectrum of (2,6-dimethylphenyl)(phenyl)methanol: interplay between conformational equilibria and vibronic effects. Physical Chemistry Chemical Physics 19:48, pages 32349-32360.
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Nobuyuki Harada. (2016) HPLC Separation of Diastereomers: Chiral Molecular Tools Useful for the Preparation of Enantiopure Compounds and Simultaneous Determination of Their Absolute Configurations. Molecules 21:10, pages 1328.
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Daniele PadulaLorenzo Di Bari & Gennaro Pescitelli. (2016) The “Case of Two Compounds with Similar Configuration but Nearly Mirror Image CD Spectra” Refuted. Reassignment of the Absolute Configuration of N -Formyl-3′,4′-dihydrospiro[indan-1,2′(1′ H )-pyridine] . The Journal of Organic Chemistry 81:17, pages 7725-7732.
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Nobuyuki Harada. 2015. Structure Elucidation in Organic Chemistry. Structure Elucidation in Organic Chemistry 393 444 .

Nobuyuki Harada. 2013. Stereoselective Synthesis of Drugs and Natural Products. Stereoselective Synthesis of Drugs and Natural Products 1 34 .

Nobuyuki Harada. (2008) Determination of absolute configurations by X-ray crystallography and1H NMR anisotropy. Chirality 20:5, pages 691-723.
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Yusuke Kasai, Akinori Sugio, Satoshi Sekiguchi, Shunsuke Kuwahara, Takatoshi Matsumoto, Masataka Watanabe, Akio Ichikawa & Nobuyuki Harada. (2007) Conformational Analysis of MαNP Esters, Powerful Chiral Resolution and1H NMR Anisotropy Tools – Aromatic Geometry and Solvent Effects on Δδ Values. European Journal of Organic Chemistry 2007:11, pages 1811-1826.
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Masashi Kosaka, Satoshi Sekiguchi, Junpei Naito, Makoto Uemura, Shunsuke Kuwahara, Masataka Watanabe, Nobuyuki Harada & Kunio Hiroi. (2005) Synthesis of enantiopure phthalides including 3-butylphthalide, a fragrance component of celery oil, and determination of their absolute configurations. Chirality 17:4, pages 218-232.
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Gabriel E. Job, Alex Shvets, William H. Pirkle, Shunsuke Kuwahara, Masashi Kosaka, Yusuke Kasai, Hiromi Taji, Kaori Fujita, Masataka Watanabe & Nobuyuki Harada. (2004) The effects of aromatic substituents on the chromatographic enantioseparation of diarylmethyl esters with the Whelk-O1 chiral stationary phase. Journal of Chromatography A 1055:1-2, pages 41-53.
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Junpei Naito, Masashi Kosaka, Takeo Sugito, Masataka Watanabe, Nobuyuki Harada & William H. Pirkle. (2003) Enantioresolution of fluorinated diphenylmethanols and determination of their absolute configurations by X‐Ray crystallographic and 1 H NMR anisotropy methods . Chirality 16:1, pages 22-35.
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Toshihiro Nishimura, Hiromi Taji & Nobuyuki Harada. (2003) Absolute configuration of the thyroid hormone analog KAT‐2003 as determined by the 1 H NMR anisotropy method with a novel chiral auxiliary, MαNP acid . Chirality 16:1, pages 13-21.
Crossref

Masashi Kosaka, Takeo Sugito, Yusuke Kasai, Shunsuke Kuwahara, Masataka Watanabe, Nobuyuki Harada, Gabriel E. Job, Alex Shvet & William H. Pirkle. (2003) Enantioresolution and absolute configurations of chiralmeta-substituted diphenylmethanols as determined by x-ray crystallographic and1H NMR anisotropy methods. Chirality 15:4, pages 324-328.
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Comparison of CD Spectra of (2-Methylphenyl)- and (2,6-Dimethylphenyl)-phenylmethanols Leads to Erroneous Absolute Configurations

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Comparison of CD Spectra of (2-Methylphenyl)- and (2,6-Dimethylphenyl)-phenylmethanols Leads to Erroneous Absolute Configurations

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